[5-benzyloxycarbonylamino-6-oxo-2-(m-tolyl)-1,6-dihydro-1-pyrimidinyl]acetic acid

Base Information

• Chemical Name: [5-benzyloxycarbonylamino-6-oxo-2-(m-tolyl)-1,6-dihydro-1-pyrimidinyl]acetic acid
• CAS No.: 184710-62-1
• Molecular Formula: C₂₁H₁₉N₃O₅
• Molecular Weight: 393.399

Synonyms:[5-benzyloxycarbonylamino-6-oxo-2-(m-tolyl)-1,6-dihydro-1-pyrimidinyl]acetic acid

Chemical Property of [5-benzyloxycarbonylamino-6-oxo-2-(m-tolyl)-1,6-dihydro-1-pyrimidinyl]acetic acid

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Technology Process of [5-benzyloxycarbonylamino-6-oxo-2-(m-tolyl)-1,6-dihydro-1-pyrimidinyl]acetic acid

There total 1 articles about [5-benzyloxycarbonylamino-6-oxo-2-(m-tolyl)-1,6-dihydro-1-pyrimidinyl]acetic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

→ [5-benzyloxycarbonylamino-6-oxo-2-(m-tolyl)-1,6-dihydro-1-pyrimidinyl]acetic acid (184710-62-1)

Guidance literature:

Reference yield: 82.0%

[5-benzyloxycarbonylamino-6-oxo-2-(m-tolyl)-1,6-dihydro-1-pyrimidinyl]acetic acid (184710-62-1) + 4-amino-4-benzyl-2,2-difluoro-3-hydroxy-N-methylbutanamide hydrochloride → 2-[5-benzyloxycarbonylamino-6-oxo-2-(m-tolyl)-1,6-dihydro-1-pyrimidinyl]-N-[1-benzyl-3,3-difluoro-2-hydroxy-3-(N-methylcarbamoyl)propyl]acetamide (339169-57-2)

Guidance literature:

With N-ethylmorpholine;; 1-hydroxybenzotriazol-hydrate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In N,N-dimethyl-formamide; at 20 ℃; for 16h;

DOI:10.1021/jm000497n

Reference yield: 73.0%

[5-benzyloxycarbonylamino-6-oxo-2-(m-tolyl)-1,6-dihydro-1-pyrimidinyl]acetic acid (184710-62-1) + ethyl 4-benzyl-4-amino-2,2-difluoro-3-hydroxybutylate hydrochloride → 2-[5-benzyloxycarbonylamino-6-oxo-2-(m-tolyl)-1,6-dihydro-1-pyrimidinyl]-N-[1-benzyl-3-(ethoxycarbonyl)-3,3-difluoro-2-hydroxypropyl]acetamide (339169-56-1)

Guidance literature:

With N-ethylmorpholine;; 1-hydroxybenzotriazol-hydrate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In N,N-dimethyl-formamide; at 20 ℃; for 16h;

DOI:10.1021/jm000497n

Downstream raw materials:

2-[5-Benzyloxycarbonylamino-6-oxo-2-(m-tolyl)-1,6-dihydro-1-pyrimidyl]-N-(1-benzyl-3,3,3-trifluoro-2-hydroxypropyl)acetamide

{1-[(1-benzyl-3-carbamoyl-3,3-difluoro-2-hydroxy-propylcarbamoyl)-methyl]-6-oxo-2-m-tolyl-1,6-dihydro-pyrimidin-5-yl}-carbamic acid benzyl ester

{1-[(1-benzyl-3-dimethylcarbamoyl-3,3-difluoro-2-hydroxy-propylcarbamoyl)-methyl]-6-oxo-2-m-tolyl-1,6-dihydro-pyrimidin-5-yl}-carbamic acid benzyl ester

2-[5-benzyloxycarbonylamino-6-oxo-2-(m-tolyl)-1,6-dihydro-1-pyrimidinyl]-N-[1-benzyl-3-(ethoxycarbonyl)-3,3-difluoro-2-hydroxypropyl]acetamide

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