1,9-bis(2'-phenylcarbamoylhydrazono-1'-ethoxycarbonylpropyl)-5,5'-diethyldipyrromethane

Base Information

Chemical Name:1,9-bis(2'-phenylcarbamoylhydrazono-1'-ethoxycarbonylpropyl)-5,5'-diethyldipyrromethane
CAS No.:1426304-24-6
Molecular Formula:C₃₉H₄₈N₈O₆
Molecular Weight:724.86
Hs Code.:

Synonyms:1,9-bis(2'-phenylcarbamoylhydrazono-1'-ethoxycarbonylpropyl)-5,5'-diethyldipyrromethane

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Chemical Property of 1,9-bis(2'-phenylcarbamoylhydrazono-1'-ethoxycarbonylpropyl)-5,5'-diethyldipyrromethane

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Technology Process of 1,9-bis(2'-phenylcarbamoylhydrazono-1'-ethoxycarbonylpropyl)-5,5'-diethyldipyrromethane

There total 3 articles about 1,9-bis(2'-phenylcarbamoylhydrazono-1'-ethoxycarbonylpropyl)-5,5'-diethyldipyrromethane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 141739-42-6
C₁₃H₁₆ClN₃O₃

: 34492-01-8
meso-diethyl-2,2'-dipyrromethane

: 1426304-24-6
1,9-bis(2'-phenylcarbamoylhydrazono-1'-ethoxycarbonylpropyl)-5,5'-diethyldipyrromethane

Guidance literature:: With sodium carbonate; In dichloromethane; water; at 20 ℃; for 3h;
DOI:10.1002/ejoc.201402944

Reference yield: 81.0%

: 141739-42-6
C₁₃H₁₆ClN₃O₃

: 34492-01-8
meso-diethyl-2,2'-dipyrromethane

: 1426304-24-6
1,9-bis(2'-phenylcarbamoylhydrazono-1'-ethoxycarbonylpropyl)-5,5'-diethyldipyrromethane

: 1-(2'-phenylcarbamoylhydrazono-1'-ethoxycarbonylpropyl)-5,5'-diethyldipyrromethane

Guidance literature:: With sodium carbonate; In dichloromethane; water; at 20 ℃; for 2h;
DOI:10.1002/ejoc.201402944

Reference yield:

: 96-22-0
pentan-3-one

: 1426304-24-6
1,9-bis(2'-phenylcarbamoylhydrazono-1'-ethoxycarbonylpropyl)-5,5'-diethyldipyrromethane

Guidance literature:: Multi-step reaction with 2 steps

1: water

2: sodium carbonate / dichloromethane / 80 h / 20 °C

With sodium carbonate; In dichloromethane; water;
DOI:10.1016/j.tetlet.2013.01.032