1,3,5-tris{3-[(S)-(-)-4-(3,7-dimethyl)octyloxyphenyl]isoxazol-5-yl}benzene

Base Information

Chemical Name:1,3,5-tris{3-[(S)-(-)-4-(3,7-dimethyl)octyloxyphenyl]isoxazol-5-yl}benzene
CAS No.:1009641-23-9
Molecular Formula:C₆₃H₈₁N₃O₆
Molecular Weight:976.353
Hs Code.:

Synonyms:1,3,5-tris{3-[(S)-(-)-4-(3,7-dimethyl)octyloxyphenyl]isoxazol-5-yl}benzene

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1,3,5-tris{3-[(S)-(-)-4-(3,7-dimethyl)octyloxyphenyl]isoxazol-5-yl}benzene

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Technology Process of 1,3,5-tris{3-[(S)-(-)-4-(3,7-dimethyl)octyloxyphenyl]isoxazol-5-yl}benzene

There total 3 articles about 1,3,5-tris{3-[(S)-(-)-4-(3,7-dimethyl)octyloxyphenyl]isoxazol-5-yl}benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 22.0%

: C₁₇H₂₆ClNO₂

: 7567-63-7
1,3,5-Triethynylbenzene

: 1009641-23-9
1,3,5-tris{3-[(S)-(-)-4-(3,7-dimethyl)octyloxyphenyl]isoxazol-5-yl}benzene

Guidance literature:: With triethylamine; In dichloromethane; at 20 ℃; for 48h;
DOI:10.1039/b715871h

Reference yield: 22.0%

: 7567-63-7
1,3,5-Triethynylbenzene

: 1009641-24-0
(S)-4-(3,7-dimethyloctyloxy)benzohydroximoyl chloride

: 1009641-23-9
1,3,5-tris{3-[(S)-(-)-4-(3,7-dimethyl)octyloxyphenyl]isoxazol-5-yl}benzene

Guidance literature:: With triethylamine; In dichloromethane; at 20 ℃; for 48h; Inert atmosphere;
DOI:10.1021/jo200766u

Reference yield:

: 1004781-43-4
(S)-4-(3,7-dimethyloctyloxy)benzaldehyde

: 1009641-23-9
1,3,5-tris{3-[(S)-(-)-4-(3,7-dimethyl)octyloxyphenyl]isoxazol-5-yl}benzene

Guidance literature:: Multi-step reaction with 3 steps

1: hydroxylamine hydrochloride; sodium hydroxide / ethanol; water / 1 h / 20 °C / Inert atmosphere

2: N-chloro-succinimide / N,N-dimethyl-formamide / 1 h / 20 °C / Inert atmosphere

3: triethylamine / dichloromethane / 48 h / 20 °C / Inert atmosphere

With N-chloro-succinimide; hydroxylamine hydrochloride; triethylamine; sodium hydroxide; In ethanol; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1021/jo200766u