C₅₄H₁₀₂O₉Si₄

Base Information

Chemical Name:C₅₄H₁₀₂O₉Si₄
CAS No.:1422462-94-9
Molecular Formula:C₅₄H₁₀₂O₉Si₄
Molecular Weight:1007.74
Hs Code.:

C<sub>54</sub>H<sub>102</sub>O<sub>9</sub>Si<sub>4</sub>

Synonyms:C₅₄H₁₀₂O₉Si₄

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Chemical Property of C₅₄H₁₀₂O₉Si₄

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Technology Process of C₅₄H₁₀₂O₉Si₄

There total 26 articles about C₅₄H₁₀₂O₉Si₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 1422463-34-0
C₄₈H₈₈O₉Si₃

: 79271-56-0
triethylsilyl trifluoromethyl sulfonate

: 1422462-94-9
C₅₄H₁₀₂O₉Si₄

: 1422462-93-8
C₅₇H₁₀₈O₉Si₄

Guidance literature:: With triethylamine; In dichloromethane; at -78 ℃; for 0.333333h; Overall yield = 95 %; diastereoselective reaction; Inert atmosphere;
DOI:10.1021/jo3026077

Reference yield:

: 1422462-85-8
C₂₆H₄₈O₅Si₂

: 1422462-94-9
C₅₄H₁₀₂O₉Si₄

Guidance literature:: Multi-step reaction with 2 steps

1.1: lithium diisopropyl amide / tetrahydrofuran; diethyl ether / 0.33 h / -78 °C / Inert atmosphere

1.2: 0.33 h / -78 °C / Inert atmosphere

2.1: triethylamine / dichloromethane / 0.33 h / -78 °C / Inert atmosphere

With triethylamine; lithium diisopropyl amide; In tetrahydrofuran; diethyl ether; dichloromethane;
DOI:10.1021/jo3026077

Reference yield:

: C₂₉H₄₈O₅Si

: 1422462-94-9
C₅₄H₁₀₂O₉Si₄

Guidance literature:: Multi-step reaction with 3 steps

1.1: water; sodium periodate / tetrahydrofuran; diethyl ether / 2 h / 20 °C

2.1: lithium diisopropyl amide / tetrahydrofuran; diethyl ether / 0.33 h / -78 °C / Inert atmosphere

2.2: 0.33 h / -78 °C / Inert atmosphere

3.1: triethylamine / dichloromethane / 0.33 h / -78 °C / Inert atmosphere

With sodium periodate; water; triethylamine; lithium diisopropyl amide; In tetrahydrofuran; diethyl ether; dichloromethane;
DOI:10.1021/jo3026077