N-(6-methoxy-2H-<1,2,4>thiadiazolo<3',2':2,3>thiazolo<5,4-b>pyridin-2-ylidene)-p-toluylamine

Base Information

Chemical Name:N-(6-methoxy-2H-<1,2,4>thiadiazolo<3',2':2,3>thiazolo<5,4-b>pyridin-2-ylidene)-p-toluylamine
CAS No.:128530-43-8
Molecular Formula:C₁₆H₁₂N₄O₂S₂
Molecular Weight:356.429
Hs Code.:

Synonyms:N-(6-methoxy-2H-<1,2,4>thiadiazolo<3',2':2,3>thiazolo<5,4-b>pyridin-2-ylidene)-p-toluylamine

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Chemical Property of N-(6-methoxy-2H-<1,2,4>thiadiazolo<3',2':2,3>thiazolo<5,4-b>pyridin-2-ylidene)-p-toluylamine

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Technology Process of N-(6-methoxy-2H-<1,2,4>thiadiazolo<3',2':2,3>thiazolo<5,4-b>pyridin-2-ylidene)-p-toluylamine

There total 4 articles about N-(6-methoxy-2H-<1,2,4>thiadiazolo<3',2':2,3>thiazolo<5,4-b>pyridin-2-ylidene)-p-toluylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

: 128530-35-8
N-p-toluyl-N'-(6-methoxythiazolo<5,4-b>pyridin-2-yl)thiourea

: 128530-43-8
N-(6-methoxy-2H-<1,2,4>thiadiazolo<3',2':2,3>thiazolo<5,4-b>pyridin-2-ylidene)-p-toluylamine

Guidance literature:: With phosphorus pentachloride; In trichlorophosphate; for 4h; Heating;

Reference yield:

: 13797-77-8
5-methoxythiazolo[5,4-b]pyridin-2-amine

: 128530-43-8
N-(6-methoxy-2H-<1,2,4>thiadiazolo<3',2':2,3>thiazolo<5,4-b>pyridin-2-ylidene)-p-toluylamine

Guidance literature:: Multi-step reaction with 2 steps

1: 76 percent / acetone / 5 h / Heating

2: 69 percent / PCl₅ / POCl₃ / 4 h / Heating

With phosphorus pentachloride; In acetone; trichlorophosphate;

Reference yield:

: 16794-68-6
4-methylbenzoyl isothiocyanate

: 128530-43-8
N-(6-methoxy-2H-<1,2,4>thiadiazolo<3',2':2,3>thiazolo<5,4-b>pyridin-2-ylidene)-p-toluylamine

Guidance literature:: Multi-step reaction with 2 steps

1: 76 percent / acetone / 5 h / Heating

2: 69 percent / PCl₅ / POCl₃ / 4 h / Heating

With phosphorus pentachloride; In acetone; trichlorophosphate;