1-((4R,6S)-6-(2-(benzyloxy)ethyl)-2,2-dimethyl-1,3-dioxan-4-yl)propan-2-one

Base Information

Chemical Name:1-((4R,6S)-6-(2-(benzyloxy)ethyl)-2,2-dimethyl-1,3-dioxan-4-yl)propan-2-one
CAS No.:1171867-50-7
Molecular Formula:C₁₈H₂₆O₄
Molecular Weight:306.402
Hs Code.:

Synonyms:1-((4R,6S)-6-(2-(benzyloxy)ethyl)-2,2-dimethyl-1,3-dioxan-4-yl)propan-2-one

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-((4R,6S)-6-(2-(benzyloxy)ethyl)-2,2-dimethyl-1,3-dioxan-4-yl)propan-2-one

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Technology Process of 1-((4R,6S)-6-(2-(benzyloxy)ethyl)-2,2-dimethyl-1,3-dioxan-4-yl)propan-2-one

There total 1 articles about 1-((4R,6S)-6-(2-(benzyloxy)ethyl)-2,2-dimethyl-1,3-dioxan-4-yl)propan-2-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 171524-04-2
(4R,6S)-4-allyl-6-(2-(benzyloxy)ethyl)-2,2-dimethyl-1,3-dioxane

: 1171867-50-7
1-((4R,6S)-6-(2-(benzyloxy)ethyl)-2,2-dimethyl-1,3-dioxan-4-yl)propan-2-one

Guidance literature:: With oxygen; copper(l) chloride; palladium dichloride; In water; N,N-dimethyl-formamide; for 4h;
DOI:10.1016/j.tetlet.2009.03.019

Reference yield:

: 1171867-50-7
1-((4R,6S)-6-(2-(benzyloxy)ethyl)-2,2-dimethyl-1,3-dioxan-4-yl)propan-2-one

: C₈₈H₁₁₀O₆Si₄

: C₁₀₆H₁₃₆O₁₀Si₄

: C₁₀₆H₁₃₆O₁₀Si₄

Guidance literature:: 1-((4R,6S)-6-(2-(benzyloxy)ethyl)-2,2-dimethyl-1,3-dioxan-4-yl)propan-2-one; With di-n-butylboryl trifluoromethanesulfonate; N-ethyl-N,N-diisopropylamine; In diethyl ether; at -78 ℃; for 1h;

C₈₈H₁₁₀O₆Si₄; In diethyl ether; dichloromethane; at -78 ℃; for 17h; optical yield given as %de;
DOI:10.1016/j.tetlet.2009.03.019