(R(S),R)-N-tert-butanesulfinyl-5-chloro-2-phenylpentylamine

Base Information

Chemical Name:(R(S),R)-N-tert-butanesulfinyl-5-chloro-2-phenylpentylamine
CAS No.:1258939-74-0
Molecular Formula:C₁₅H₂₄ClNOS
Molecular Weight:301.881
Hs Code.:

Synonyms:(R(S),R)-N-tert-butanesulfinyl-5-chloro-2-phenylpentylamine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (R(S),R)-N-tert-butanesulfinyl-5-chloro-2-phenylpentylamine

Chemical Property:

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Technology Process of (R(S),R)-N-tert-butanesulfinyl-5-chloro-2-phenylpentylamine

There total 3 articles about (R(S),R)-N-tert-butanesulfinyl-5-chloro-2-phenylpentylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: (R(S),R)-methyl N-tert-butanesulfinyl-5-chloro-2-phenylpentanimidate

: 1258939-74-0
(R(S),R)-N-tert-butanesulfinyl-5-chloro-2-phenylpentylamine

Guidance literature:: With sodium tetrahydroborate; In tetrahydrofuran; methanol; Reflux;
DOI:10.1021/jo1020807

Reference yield:

: 101-41-7
benzeneacetic acid methyl ester

: 1258939-74-0
(R(S),R)-N-tert-butanesulfinyl-5-chloro-2-phenylpentylamine

Guidance literature:: Multi-step reaction with 3 steps

1.1: toluene-4-sulfonic acid / neat (no solvent)

2.1: lithium hexamethyldisilazane / tetrahydrofuran / -78 °C

2.2: -78 - 0 °C

3.1: sodium tetrahydroborate / tetrahydrofuran; methanol / Reflux

With sodium tetrahydroborate; toluene-4-sulfonic acid; lithium hexamethyldisilazane; In tetrahydrofuran; methanol;
DOI:10.1021/jo1020807

Reference yield:

: 817576-00-4
(R(S))-methyl N-tert-butanesulfinylphenylacetimidate

: 1258939-74-0
(R(S),R)-N-tert-butanesulfinyl-5-chloro-2-phenylpentylamine

Guidance literature:: Multi-step reaction with 2 steps

1.1: lithium hexamethyldisilazane / tetrahydrofuran / -78 °C

1.2: -78 - 0 °C

2.1: sodium tetrahydroborate / tetrahydrofuran; methanol / Reflux

With sodium tetrahydroborate; lithium hexamethyldisilazane; In tetrahydrofuran; methanol;
DOI:10.1021/jo1020807