tris(pentafluorophenyl)borane-triphenylphosphine

Base Information

• Chemical Name: tris(pentafluorophenyl)borane-triphenylphosphine
• CAS No.: 2317-39-7
• Molecular Formula: C₃₆H₁₅BF₁₅P
• Molecular Weight: 774.276

Synonyms:tris(pentafluorophenyl)borane-triphenylphosphine

Chemical Property of tris(pentafluorophenyl)borane-triphenylphosphine

Chemical Property:

Purity/Quality:

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Technology Process of tris(pentafluorophenyl)borane-triphenylphosphine

There total 6 articles about tris(pentafluorophenyl)borane-triphenylphosphine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

tris(pentafluorophenyl)borate (1109-15-5) + triphenylphosphine (603-35-0) → tris(pentafluorophenyl)borane-triphenylphosphine (2317-39-7)

Guidance literature:

In pentane; Ar-atmosphere; pptn. on refluxing, stirring (room temp., 1 h); filtering, washing (pentane), drying (vac.); elem. anal.;

DOI:10.1021/om981033e

Reference yield:

phenyl(triphenylphosphine)[diphenylbis((trimethylsilyl)imino)phosphorato]nickel (827319-45-9) + tris(pentafluorophenyl)borate (1109-15-5) → tris(pentafluorophenyl)borane-triphenylphosphine (2317-39-7)

Guidance literature:

With 1-hexene; In further solvent(s); byproducts: 2-hexene, 3-hexene; under N2; in NMR tube; soln. of B(C6F5)3 in C6D6 added to soln. of Ni complex in C6D6-hexene-1; not isolated; monitored by (1)H, (31)P and (19)F NMR spectra;

DOI:10.1021/om051103z

Reference yield:

Si((CH2)11CH3)2(C4HSC6H3N2S)2(B(C6F5)3)2 (1176202-73-5) + triphenylphosphine (603-35-0) → tris(pentafluorophenyl)borane-triphenylphosphine (2317-39-7)

Guidance literature:

In not given; byproducts: Si(dodecyl)2(C4HSC6H3N2S)2; addn. of excess phosphine; detected by NMR;

DOI:10.1021/ja902789w

upstream raw materials:

tris(pentafluorophenyl)borate

triphenylphosphine

phenyl(triphenylphosphine)[diphenylbis((trimethylsilyl)imino)phosphorato]nickel

Si((CH₂)11CH₃)2(C₄HSC₆H₃N₂S)2(B(C₆F₅)3)2

Downstream raw materials:

Ph₃P(C₆F₄)BF(C₆F₅)2

E-Ph₃P(Ph)C=C(H)B(C₆F₅)3

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