biphenyl-2-ylcarbamic acid 1-{2-[(3-chlorocarbonylphenyl)methyl-carbamoyl]ethyl}piperidin-4-yl ester

Base Information

Chemical Name:biphenyl-2-ylcarbamic acid 1-{2-[(3-chlorocarbonylphenyl)methyl-carbamoyl]ethyl}piperidin-4-yl ester
CAS No.:1253582-63-6
Molecular Formula:C₂₉H₃₀ClN₃O₄
Molecular Weight:520.028
Hs Code.:

Synonyms:biphenyl-2-ylcarbamic acid 1-{2-[(3-chlorocarbonylphenyl)methyl-carbamoyl]ethyl}piperidin-4-yl ester

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Chemical Property of biphenyl-2-ylcarbamic acid 1-{2-[(3-chlorocarbonylphenyl)methyl-carbamoyl]ethyl}piperidin-4-yl ester

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Technology Process of biphenyl-2-ylcarbamic acid 1-{2-[(3-chlorocarbonylphenyl)methyl-carbamoyl]ethyl}piperidin-4-yl ester

There total 4 articles about biphenyl-2-ylcarbamic acid 1-{2-[(3-chlorocarbonylphenyl)methyl-carbamoyl]ethyl}piperidin-4-yl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1253582-41-0
3-({3-[4-(biphenyl-2-ylcarbamoyloxy)piperidin-1-yl]propionyl}methylamino)benzoic acid

: 1253582-63-6
biphenyl-2-ylcarbamic acid 1-{2-[(3-chlorocarbonylphenyl)methyl-carbamoyl]ethyl}piperidin-4-yl ester

Guidance literature:: With thionyl chloride; at 20 ℃; for 1h;

Reference yield:

: 4518-10-9
Methyl 3-aminobenzoate

: 1253582-63-6
biphenyl-2-ylcarbamic acid 1-{2-[(3-chlorocarbonylphenyl)methyl-carbamoyl]ethyl}piperidin-4-yl ester

Guidance literature:: Multi-step reaction with 5 steps

1.1: acetic anhydride / 1 h / 20 °C

2.1: sodium hydrogencarbonate / dichloromethane / 0 °C

3.1: ethanol / 90 °C

4.1: water; lithium hydroxide / acetonitrile / 20 °C

4.2: pH 5

5.1: thionyl chloride / 1 h / 20 °C

With thionyl chloride; water; acetic anhydride; sodium hydrogencarbonate; lithium hydroxide; In ethanol; dichloromethane; acetonitrile;

Reference yield:

: 1253582-39-6
methyl 3-(N-methylacrylamido)benzoate

: 1253582-63-6
biphenyl-2-ylcarbamic acid 1-{2-[(3-chlorocarbonylphenyl)methyl-carbamoyl]ethyl}piperidin-4-yl ester

Guidance literature:: Multi-step reaction with 3 steps

1.1: ethanol / 90 °C

2.1: water; lithium hydroxide / acetonitrile / 20 °C

2.2: pH 5

3.1: thionyl chloride / 1 h / 20 °C

With thionyl chloride; water; lithium hydroxide; In ethanol; acetonitrile;