Technology Process of C47H46N14O9S7
There total 8 articles about C47H46N14O9S7 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
hydrogenchloride;
In
dichloromethane;
at 0 ℃;
for 2.16667h;
- Guidance literature:
-
C54H56N14O12S7;
With
potassium carbonate;
In
methanol;
at 22 ℃;
for 2h;
With
hydrogenchloride;
In
dichloromethane;
at 0 ℃;
for 2.16667h;
DOI:10.1021/jm200938f
- Guidance literature:
-
Multi-step reaction with 7 steps
1.1: water; sodium hydroxide / tetrahydrofuran / 1.5 h / 60 °C
2.1: chloroformic acid ethyl ester; triethylamine / acetone / 1 h
2.2: 1.33 h / 60 °C
3.1: 2 h / 80 °C
4.1: pyridine; dmap / 3 h
5.1: hydrogenchloride / dichloromethane
6.1: methanol / 0.08 h / 0 °C
7.1: potassium carbonate / methanol / 2 h / 22 °C
7.2: 2.17 h / 0 °C
With
pyridine; hydrogenchloride; dmap; water; chloroformic acid ethyl ester; potassium carbonate; triethylamine; sodium hydroxide;
In
tetrahydrofuran; methanol; dichloromethane; acetone;
DOI:10.1021/jm200938f