diethyl N-<4-ethyl>-N-methylamino>benzoyl>-L-glutamate

Base Information

Chemical Name:diethyl N-<4-ethyl>-N-methylamino>benzoyl>-L-glutamate
CAS No.:107716-34-7
Molecular Formula:C₂₄H₃₄N₆O₆
Molecular Weight:502.571
Hs Code.:

diethyl N-<4-<N-<2-<N-(2-amino-4-oxo-6-methylpyrimidin-5-yl)amino>ethyl>-N-methylamino>benzoyl>-L-glutamate

Synonyms:diethyl N-<4-ethyl>-N-methylamino>benzoyl>-L-glutamate

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Chemical Property of diethyl N-<4-ethyl>-N-methylamino>benzoyl>-L-glutamate

Chemical Property:

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Technology Process of diethyl N-<4-ethyl>-N-methylamino>benzoyl>-L-glutamate

There total 6 articles about diethyl N-<4-ethyl>-N-methylamino>benzoyl>-L-glutamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 20.0%

: 4214-86-2
2,5-diamino-4-oxo-6-methyl pyrimidine

: 107716-32-5
diethyl N-<4-benzoyl>-L-glutamate

: 107716-34-7
diethyl N-<4-ethyl>-N-methylamino>benzoyl>-L-glutamate

Guidance literature:: In N,N-dimethyl-formamide; at 90 - 100 ℃; for 24h;
DOI:10.1021/jm00119a012

Reference yield:

: 13726-52-8
diethyl N-(p-aminobenzoyl)-L-glutamate

: 107716-34-7
diethyl N-<4-ethyl>-N-methylamino>benzoyl>-L-glutamate

Guidance literature:: Multi-step reaction with 6 steps

1: 94 percent / sodium cyanoborohydride, bromocresol green, acetic acid / ethanol / 48 h / Ambient temperature

2: 91 percent / sodium cyanoborohydride, bromocresol green, aq. acetic acid / acetonitrile / 1 h / Ambient temperature

3: 80 percent / hydrogen, HCl / palladium on carbon / ethanol / 3 h / 2482.3 Torr

4: aq. acetic acid / 1.) 0 deg C, 2.) room temperature, 17 h

5: 80 percent / pyridine / 1 h / Ambient temperature

6: 20 percent / dimethylformamide / 24 h / 90 - 100 °C

With hydrogenchloride; hydrogen; bromocresol green; sodium cyanoborohydride; acetic acid; palladium on activated charcoal; In pyridine; ethanol; acetic acid; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1021/jm00119a012

Reference yield:

: 70280-70-5
diethyl N--L-glutamate

: 107716-34-7
diethyl N-<4-ethyl>-N-methylamino>benzoyl>-L-glutamate

Guidance literature:: Multi-step reaction with 5 steps

1: 91 percent / sodium cyanoborohydride, bromocresol green, aq. acetic acid / acetonitrile / 1 h / Ambient temperature

2: 80 percent / hydrogen, HCl / palladium on carbon / ethanol / 3 h / 2482.3 Torr

3: aq. acetic acid / 1.) 0 deg C, 2.) room temperature, 17 h

4: 80 percent / pyridine / 1 h / Ambient temperature

5: 20 percent / dimethylformamide / 24 h / 90 - 100 °C

With hydrogenchloride; hydrogen; bromocresol green; sodium cyanoborohydride; acetic acid; palladium on activated charcoal; In pyridine; ethanol; acetic acid; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1021/jm00119a012