2,3-di-O-benzoyl-4,6-O-di-tert-butylsilylene-α-D-galactopyranosyl trichloroacetimidate

Base Information

Chemical Name:2,3-di-O-benzoyl-4,6-O-di-tert-butylsilylene-α-D-galactopyranosyl trichloroacetimidate
CAS No.:916596-71-9
Molecular Formula:C₃₀H₃₆Cl₃NO₈Si
Molecular Weight:673.062
Hs Code.:

Synonyms:2,3-di-O-benzoyl-4,6-O-di-tert-butylsilylene-α-D-galactopyranosyl trichloroacetimidate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2,3-di-O-benzoyl-4,6-O-di-tert-butylsilylene-α-D-galactopyranosyl trichloroacetimidate

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Technology Process of 2,3-di-O-benzoyl-4,6-O-di-tert-butylsilylene-α-D-galactopyranosyl trichloroacetimidate

There total 11 articles about 2,3-di-O-benzoyl-4,6-O-di-tert-butylsilylene-α-D-galactopyranosyl trichloroacetimidate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 2,3-di-O-benzoyl-4,6-O-di-tert-butylsilanediyl-α-D-galactopyranose

: 545-06-2
trichloroacetonitrile

: 916596-71-9
2,3-di-O-benzoyl-4,6-O-di-tert-butylsilylene-α-D-galactopyranosyl trichloroacetimidate

Guidance literature:: With 1,8-diazabicyclo[5.4.0]undec-7-ene; In dichloromethane; at 20 ℃; for 1h;
DOI:10.1002/chem.200600832

Reference yield: 98.0%

: 2,3-di-O-benzoyl-4,6-O-di-tert-butylsilanediyl-D-galactopyranose

: 545-06-2
trichloroacetonitrile

: 916596-71-9
2,3-di-O-benzoyl-4,6-O-di-tert-butylsilylene-α-D-galactopyranosyl trichloroacetimidate

Guidance literature:: With 1,8-diazabicyclo[5.4.0]undec-7-ene; In dichloromethane;
DOI:10.1055/s-2006-949649

Reference yield:

: 2,3-di-O-benzoyl-4,6-O-di-tert-butylsilanediyl-D-galactopyranose

: 545-06-2
trichloroacetonitrile

: 916596-71-9
2,3-di-O-benzoyl-4,6-O-di-tert-butylsilylene-α-D-galactopyranosyl trichloroacetimidate

: 2,3-di-O-benzoyl-4,6-O-di-tert-butylsilylene-D-galactopyranosyl trichloroacetimidate

Guidance literature:: With 1,8-diazabicyclo[5.4.0]undec-7-ene; In dichloromethane; at 0 ℃; for 6h; Overall yield = 93 percent; Overall yield = 711 mg; Inert atmosphere;
DOI:10.1039/c9ra05797h