(E)-N-phenyl-2-(quinolin-2-ylmethylene)hydrazinecarbothioamide

Base Information

• Chemical Name: (E)-N-phenyl-2-(quinolin-2-ylmethylene)hydrazinecarbothioamide
• CAS No.: 1313215-50-7
• Molecular Formula: C₁₇H₁₄N₄S
• Molecular Weight: 306.391
• Mol file: 1313215-50-7.mol

Synonyms:(E)-N-phenyl-2-(quinolin-2-ylmethylene)hydrazinecarbothioamide

Chemical Property of (E)-N-phenyl-2-(quinolin-2-ylmethylene)hydrazinecarbothioamide

Chemical Property:

Purity/Quality:

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MSDS Files:

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Technology Process of (E)-N-phenyl-2-(quinolin-2-ylmethylene)hydrazinecarbothioamide

There total 1 articles about (E)-N-phenyl-2-(quinolin-2-ylmethylene)hydrazinecarbothioamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

quinoline 2-carbaldehyde (5470-96-2) + 4-Phenyl-3-thiosemicarbazide (5351-69-9) → (E)-N-phenyl-2-(quinolin-2-ylmethylene)hydrazinecarbothioamide (1313215-50-7)

Guidance literature:

With acetic acid; In ethanol; at 83 ℃; for 0.166667h; Microwave irradiation;

DOI:10.1016/j.bmcl.2012.07.030

Reference yield: 78.0%

cobalt(II) chloride hexahydrate + (E)-N-phenyl-2-(quinolin-2-ylmethylene)hydrazinecarbothioamide (1313215-50-7) → [Co(PQTS)2]Cl·H2O

Guidance literature:

In ethanol; at 75 ℃; for 1h;

DOI:10.1016/j.molstruc.2018.04.074

upstream raw materials:

quinoline 2-carbaldehyde

4-Phenyl-3-thiosemicarbazide