Technology Process of 2-amino-4,6-diisopropoxybenzoic acid
There total 7 articles about 2-amino-4,6-diisopropoxybenzoic acid which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
4,6-diisopropoxy-1H-indole-2,3-dione;
With
dihydrogen peroxide; potassium hydroxide;
In
water;
at 0 - 70 ℃;
for 0.5h;
With
hydrogenchloride;
In
water;
at 0 ℃;
for 4h;
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: 1 h / Reflux
2.1: potassium hydroxide; dihydrogen peroxide / water / 0.5 h / 70 °C
2.2: 0 °C / pH 4
With
dihydrogen peroxide; potassium hydroxide;
In
water;
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: potassium carbonate / N,N-dimethyl-formamide / 14 h / 20 °C
2.1: methanol; lithium hydroxide / tetrahydrofuran; water
3.1: triethylamine; diphenyl phosphoryl azide / 1,4-dioxane; tert-butyl alcohol / 16 h / Reflux
4.1: 0.5 h / Reflux
5.1: 1 h / Reflux
6.1: potassium hydroxide; dihydrogen peroxide / water / 0.5 h / 70 °C
6.2: 0 °C / pH 4
With
methanol; diphenyl phosphoryl azide; dihydrogen peroxide; potassium carbonate; triethylamine; potassium hydroxide; lithium hydroxide;
In
tetrahydrofuran; 1,4-dioxane; water; N,N-dimethyl-formamide; tert-butyl alcohol;
