6-(2-chloro-4-iodoanilino)-N-(2-vinyloxyethoxy)-5-methyl-4-oxo-4,5-dihydrofuro[3,2-c]pyridin-7-amide

Base Information

Chemical Name:6-(2-chloro-4-iodoanilino)-N-(2-vinyloxyethoxy)-5-methyl-4-oxo-4,5-dihydrofuro[3,2-c]pyridin-7-amide
CAS No.:1400819-02-4
Molecular Formula:C₁₉H₁₇ClIN₃O₅
Molecular Weight:529.719
Hs Code.:

Synonyms:6-(2-chloro-4-iodoanilino)-N-(2-vinyloxyethoxy)-5-methyl-4-oxo-4,5-dihydrofuro[3,2-c]pyridin-7-amide

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Chemical Property of 6-(2-chloro-4-iodoanilino)-N-(2-vinyloxyethoxy)-5-methyl-4-oxo-4,5-dihydrofuro[3,2-c]pyridin-7-amide

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Technology Process of 6-(2-chloro-4-iodoanilino)-N-(2-vinyloxyethoxy)-5-methyl-4-oxo-4,5-dihydrofuro[3,2-c]pyridin-7-amide

There total 6 articles about 6-(2-chloro-4-iodoanilino)-N-(2-vinyloxyethoxy)-5-methyl-4-oxo-4,5-dihydrofuro[3,2-c]pyridin-7-amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 391212-29-6
O-(2-vinyloxyethyl)hydroxylamine

: 1392272-33-1
methyl 6-(2-chloro-4-iodophenylamino)-5-methyl-4-oxo-4,5-dihydrofuro[3,2-c]pyridine-7-carboxylate

: 1400819-02-4
6-(2-chloro-4-iodoanilino)-N-(2-vinyloxyethoxy)-5-methyl-4-oxo-4,5-dihydrofuro[3,2-c]pyridin-7-amide

Guidance literature:: With lithium hexamethyldisilazane; In tetrahydrofuran; at 0 - 20 ℃; Inert atmosphere;

Reference yield:

: 1830-54-2
3-oxopentanedioic acid dimethyl ester

: 1400819-02-4
6-(2-chloro-4-iodoanilino)-N-(2-vinyloxyethoxy)-5-methyl-4-oxo-4,5-dihydrofuro[3,2-c]pyridin-7-amide

Guidance literature:: Multi-step reaction with 3 steps

1.1: pyridine / 0 - 50 °C

2.1: sodium hydride / tetrahydrofuran; mineral oil / 0 - 20 °C

2.2: 20 °C

3.1: lithium hexamethyldisilazane / tetrahydrofuran / 0 - 20 °C / Inert atmosphere

With pyridine; sodium hydride; lithium hexamethyldisilazane; In tetrahydrofuran; mineral oil;

Reference yield:

: 162337-80-6
methyl 3-methoxycarbonylfuran-2-ylacetate

: 1400819-02-4
6-(2-chloro-4-iodoanilino)-N-(2-vinyloxyethoxy)-5-methyl-4-oxo-4,5-dihydrofuro[3,2-c]pyridin-7-amide

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium hydride / tetrahydrofuran; mineral oil / 0 - 20 °C

1.2: 20 °C

2.1: lithium hexamethyldisilazane / tetrahydrofuran / 0 - 20 °C / Inert atmosphere

With sodium hydride; lithium hexamethyldisilazane; In tetrahydrofuran; mineral oil;