11-(2-benzyloxy-1,1,1,3,3,3-hexafluoropropan-2-yl)-4-butyl-7,10-dimethoxy-[1,3]dioxolo[4,5-c]phenanthridin-5(4H)-one

Base Information

Chemical Name:11-(2-benzyloxy-1,1,1,3,3,3-hexafluoropropan-2-yl)-4-butyl-7,10-dimethoxy-[1,3]dioxolo[4,5-c]phenanthridin-5(4H)-one
CAS No.:1307741-87-2
Molecular Formula:C₃₀H₂₇F₆NO₆
Molecular Weight:611.538
Hs Code.:

Synonyms:11-(2-benzyloxy-1,1,1,3,3,3-hexafluoropropan-2-yl)-4-butyl-7,10-dimethoxy-[1,3]dioxolo[4,5-c]phenanthridin-5(4H)-one

Suppliers and Price of 11-(2-benzyloxy-1,1,1,3,3,3-hexafluoropropan-2-yl)-4-butyl-7,10-dimethoxy-[1,3]dioxolo[4,5-c]phenanthridin-5(4H)-one

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 11-(2-benzyloxy-1,1,1,3,3,3-hexafluoropropan-2-yl)-4-butyl-7,10-dimethoxy-[1,3]dioxolo[4,5-c]phenanthridin-5(4H)-one

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 11-(2-benzyloxy-1,1,1,3,3,3-hexafluoropropan-2-yl)-4-butyl-7,10-dimethoxy-[1,3]dioxolo[4,5-c]phenanthridin-5(4H)-one

There total 4 articles about 11-(2-benzyloxy-1,1,1,3,3,3-hexafluoropropan-2-yl)-4-butyl-7,10-dimethoxy-[1,3]dioxolo[4,5-c]phenanthridin-5(4H)-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 46.0%

: 1307741-84-9
N-[7-(2-benzyloxy-1,1,1,3,3,3-hexafluoropropan-2-yl)-6-methoxybenzo[d][1,3]dioxol-4-yl]-N-butyl-2-iodo-5-methoxybenzamide

: 1307741-87-2
11-(2-benzyloxy-1,1,1,3,3,3-hexafluoropropan-2-yl)-4-butyl-7,10-dimethoxy-[1,3]dioxolo[4,5-c]phenanthridin-5(4H)-one

Guidance literature:: With palladium diacetate; caesium carbonate; tricyclohexylphosphine tetrafluoroborate; In 2,4-dichlorophenoxyacetic acid dimethylamine; at 120 ℃; for 3h; Inert atmosphere;
DOI:10.1016/j.bmc.2011.03.002

Reference yield:

: 1307741-36-1
4-(butylamino)-6-methoxybenzo[d][1,3]dioxole

: 1307741-87-2
11-(2-benzyloxy-1,1,1,3,3,3-hexafluoropropan-2-yl)-4-butyl-7,10-dimethoxy-[1,3]dioxolo[4,5-c]phenanthridin-5(4H)-one

Guidance literature:: Multi-step reaction with 4 steps

1.1: toluene-4-sulfonic acid / toluene / 10 h / 120 °C / Molecular sieve

2.1: Vilsmeier reagent / dichloromethane / 1 h / 20 °C / Inert atmosphere

2.2: 3 h / 0 °C / Inert atmosphere

3.1: potassium carbonate / acetone

4.1: palladium diacetate; caesium carbonate; tricyclohexylphosphine tetrafluoroborate / 2,4-dichlorophenoxyacetic acid dimethylamine / 3 h / 120 °C / Inert atmosphere

With Vilsmeier reagent; palladium diacetate; potassium carbonate; caesium carbonate; toluene-4-sulfonic acid; tricyclohexylphosphine tetrafluoroborate; In dichloromethane; 2,4-dichlorophenoxyacetic acid dimethylamine; acetone; toluene;
DOI:10.1016/j.bmc.2011.03.002

Reference yield:

: 1307741-39-4
C₁₅H₁₇F₆NO₄

: 1307741-87-2
11-(2-benzyloxy-1,1,1,3,3,3-hexafluoropropan-2-yl)-4-butyl-7,10-dimethoxy-[1,3]dioxolo[4,5-c]phenanthridin-5(4H)-one

Guidance literature:: Multi-step reaction with 3 steps

1.1: Vilsmeier reagent / dichloromethane / 1 h / 20 °C / Inert atmosphere

1.2: 3 h / 0 °C / Inert atmosphere

2.1: potassium carbonate / acetone

3.1: palladium diacetate; caesium carbonate; tricyclohexylphosphine tetrafluoroborate / 2,4-dichlorophenoxyacetic acid dimethylamine / 3 h / 120 °C / Inert atmosphere

With Vilsmeier reagent; palladium diacetate; potassium carbonate; caesium carbonate; tricyclohexylphosphine tetrafluoroborate; In dichloromethane; 2,4-dichlorophenoxyacetic acid dimethylamine; acetone;
DOI:10.1016/j.bmc.2011.03.002