Acetic acid 2,6-bis-(2-acetoxy-5-bromo-benzyl)-4-chloro-phenyl ester

Base Information

• Chemical Name: Acetic acid 2,6-bis-(2-acetoxy-5-bromo-benzyl)-4-chloro-phenyl ester
• CAS No.: 196696-05-6
• Molecular Formula: C₂₆H₂₁Br₂ClO₆
• Molecular Weight: 624.71
• Mol file: 196696-05-6.mol

Synonyms:Acetic acid 2,6-bis-(2-acetoxy-5-bromo-benzyl)-4-chloro-phenyl ester

Chemical Property of Acetic acid 2,6-bis-(2-acetoxy-5-bromo-benzyl)-4-chloro-phenyl ester

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Acetic acid 2,6-bis-(2-acetoxy-5-bromo-benzyl)-4-chloro-phenyl ester

There total 1 articles about Acetic acid 2,6-bis-(2-acetoxy-5-bromo-benzyl)-4-chloro-phenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

4-chloro-2,6-bis[(5-bromo-2-hydroxyphenyl)methyl]phenol (71643-08-8) + acetic anhydride (108-24-7) → Acetic acid 2,6-bis-(2-acetoxy-5-bromo-benzyl)-4-chloro-phenyl ester (196696-05-6)

Guidance literature:

With sulfuric acid; for 2h;

Reference yield: 98.0%

Acetic acid 2,6-bis-(2-acetoxy-5-bromo-benzyl)-4-chloro-phenyl ester (196696-05-6) → 2-Acetoxy-1-(2-acetoxy-5-bromobenzyl)-3-(5-bromo-2-hydroxybenzyl)-5-chlorobenzene (196696-21-6)

Guidance literature:

With sodium hydroxide; In tetrahydrofuran; at 0 - 20 ℃; for 3h;

Reference yield: 75.0%

Acetic acid 2,6-bis-(2-acetoxy-5-bromo-benzyl)-4-chloro-phenyl ester (196696-05-6) → 1-{3-[3-(3-Acetyl-5-bromo-2-hydroxy-benzyl)-5-chloro-2-hydroxy-benzyl]-5-bromo-2-hydroxy-phenyl}-ethanone (196696-19-2)

Guidance literature:

With aluminium trichloride; at 150 - 155 ℃; for 0.333333h;

upstream raw materials:

4-chloro-2,6-bis[(5-bromo-2-hydroxyphenyl)methyl]phenol

acetic anhydride

Downstream raw materials:

2-Acetoxy-1-(2-acetoxy-5-bromobenzyl)-3-(5-bromo-2-hydroxybenzyl)-5-chlorobenzene

1-{3-[3-(3-Acetyl-5-bromo-2-hydroxy-benzyl)-5-chloro-2-hydroxy-benzyl]-5-bromo-2-hydroxy-phenyl}-ethanone

2,6-bis(3-carboxy-2-hydroxybenzyl)-4-chlorophenol

2,6-bis(5-bromo-3-carboxy-2-hydroxybenzyl)-4-chlorophenol