(1R,2R,3R,4S)-ethyl 4-((ethoxycarbonyl)methyl)-1-acetyl-2-(2-methoxyphenyl)-3-nitrocyclopentanecarboxylate

Base Information

Chemical Name:(1R,2R,3R,4S)-ethyl 4-((ethoxycarbonyl)methyl)-1-acetyl-2-(2-methoxyphenyl)-3-nitrocyclopentanecarboxylate
CAS No.:1041188-30-0
Molecular Formula:C₂₁H₂₇NO₈
Molecular Weight:421.447
Hs Code.:

Synonyms:(1R,2R,3R,4S)-ethyl 4-((ethoxycarbonyl)methyl)-1-acetyl-2-(2-methoxyphenyl)-3-nitrocyclopentanecarboxylate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (1R,2R,3R,4S)-ethyl 4-((ethoxycarbonyl)methyl)-1-acetyl-2-(2-methoxyphenyl)-3-nitrocyclopentanecarboxylate

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Technology Process of (1R,2R,3R,4S)-ethyl 4-((ethoxycarbonyl)methyl)-1-acetyl-2-(2-methoxyphenyl)-3-nitrocyclopentanecarboxylate

There total 1 articles about (1R,2R,3R,4S)-ethyl 4-((ethoxycarbonyl)methyl)-1-acetyl-2-(2-methoxyphenyl)-3-nitrocyclopentanecarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 65716-79-2
diethyl 5-acetylhex-2-enedioate

: 3316-24-3
1-methoxy-2-((E)-2-nitrovinyl)benzene

: 1041188-30-0
(1R,2R,3R,4S)-ethyl 4-((ethoxycarbonyl)methyl)-1-acetyl-2-(2-methoxyphenyl)-3-nitrocyclopentanecarboxylate

Guidance literature:: diethyl 5-acetylhex-2-enedioate; 1-methoxy-2-((E)-2-nitrovinyl)benzene; With (R)-(6-methoxyquinolin-4-yl)((1S,2S,4S,5R)-5-vinylquinuclidin-2-yl)methanamine; In diethyl ether; at 22 ℃; for 24h;

for 6h; optical yield given as %ee; enantioselective reaction; Neat (no solvent);
DOI:10.1021/ol801246m