methyl (1S,4aS,8aR)-5-(2-{2,5-bis[(E)-styryl]-furan-3-yl}ethyl)-1,4a,6-trimethyl-1,2,3,4,4a,7,8,8a-octahydronaphthalene-1-carboxylate

Base Information

Chemical Name:methyl (1S,4aS,8aR)-5-(2-{2,5-bis[(E)-styryl]-furan-3-yl}ethyl)-1,4a,6-trimethyl-1,2,3,4,4a,7,8,8a-octahydronaphthalene-1-carboxylate
CAS No.:1311993-12-0
Molecular Formula:C₃₇H₄₂O₃
Molecular Weight:534.739
Hs Code.:

Synonyms:methyl (1S,4aS,8aR)-5-(2-{2,5-bis[(E)-styryl]-furan-3-yl}ethyl)-1,4a,6-trimethyl-1,2,3,4,4a,7,8,8a-octahydronaphthalene-1-carboxylate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methyl (1S,4aS,8aR)-5-(2-{2,5-bis[(E)-styryl]-furan-3-yl}ethyl)-1,4a,6-trimethyl-1,2,3,4,4a,7,8,8a-octahydronaphthalene-1-carboxylate

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Technology Process of methyl (1S,4aS,8aR)-5-(2-{2,5-bis[(E)-styryl]-furan-3-yl}ethyl)-1,4a,6-trimethyl-1,2,3,4,4a,7,8,8a-octahydronaphthalene-1-carboxylate

There total 3 articles about methyl (1S,4aS,8aR)-5-(2-{2,5-bis[(E)-styryl]-furan-3-yl}ethyl)-1,4a,6-trimethyl-1,2,3,4,4a,7,8,8a-octahydronaphthalene-1-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

: 100-42-5,25038-60-2,25247-68-1,28213-80-1,28325-75-9,79637-11-9,9003-53-6
styrene

: 1122507-27-0
phlomisoic acid methyl ester

: 1311993-12-0
methyl (1S,4aS,8aR)-5-(2-{2,5-bis[(E)-styryl]-furan-3-yl}ethyl)-1,4a,6-trimethyl-1,2,3,4,4a,7,8,8a-octahydronaphthalene-1-carboxylate

Guidance literature:: With oxygen; copper diacetate; palladium diacetate; propionic acid; p-benzoquinone; In diethyl ether; at 35 ℃; for 10h; stereoselective reaction;
DOI:10.1134/S107042801104021X

Reference yield: 7.0%

: 100-42-5,25038-60-2,25247-68-1,28213-80-1,28325-75-9,79637-11-9,9003-53-6
styrene

: 1122507-27-0
phlomisoic acid methyl ester

: 1311993-12-0
methyl (1S,4aS,8aR)-5-(2-{2,5-bis[(E)-styryl]-furan-3-yl}ethyl)-1,4a,6-trimethyl-1,2,3,4,4a,7,8,8a-octahydronaphthalene-1-carboxylate

: 1515848-26-6
methyl (1S,4aS,8aR)-5-(2-{2-[(E)-styryl]furan-3-yl}ethyl)-1,4a,6-trimethyl-1,2,3,4,4a,7,8,8a-octahydronaphthalene-1-carboxylate

Guidance literature:: With oxygen; copper diacetate; palladium diacetate; p-benzoquinone; In propionic acid; N,N-dimethyl-formamide; at 35 ℃; for 10h; stereoselective reaction;
DOI:10.1134/S1070428013110225

Reference yield:

: 100-42-5,25038-60-2,25247-68-1,28213-80-1,28325-75-9,79637-11-9,9003-53-6
styrene

: 1122507-27-0
phlomisoic acid methyl ester

: 1311993-12-0
methyl (1S,4aS,8aR)-5-(2-{2,5-bis[(E)-styryl]-furan-3-yl}ethyl)-1,4a,6-trimethyl-1,2,3,4,4a,7,8,8a-octahydronaphthalene-1-carboxylate

: 1515848-24-4
methyl (1S,4aS,8aR)-5-{2-[2-(1-phenylvinyl)furan-3-yl]ethyl}-1,4a,6-trimethyl-1,2,3,4,4a,7,8,8a-octahydronaphthalene-1-carboxylate

: 1515848-26-6
methyl (1S,4aS,8aR)-5-(2-{2-[(E)-styryl]furan-3-yl}ethyl)-1,4a,6-trimethyl-1,2,3,4,4a,7,8,8a-octahydronaphthalene-1-carboxylate

Guidance literature:: With oxygen; copper diacetate; palladium diacetate; p-benzoquinone; In propionic acid; acetonitrile; at 35 ℃; for 10h; stereoselective reaction;
DOI:10.1134/S1070428013110225