phenyl 2,3,4-tri-O-benzyl-6-O-[2-[(4-phenylbenzyl)oxycarbonyl]benzoyl]-1-thio-α-D-glucopyranoside

Base Information

• Chemical Name: phenyl 2,3,4-tri-O-benzyl-6-O-[2-[(4-phenylbenzyl)oxycarbonyl]benzoyl]-1-thio-α-D-glucopyranoside
• CAS No.: 848866-41-1
• Molecular Formula: C₅₄H₄₈O₈S
• Molecular Weight: 857.036

Synonyms:phenyl 2,3,4-tri-O-benzyl-6-O-[2-[(4-phenylbenzyl)oxycarbonyl]benzoyl]-1-thio-α-D-glucopyranoside

Chemical Property of phenyl 2,3,4-tri-O-benzyl-6-O-[2-[(4-phenylbenzyl)oxycarbonyl]benzoyl]-1-thio-α-D-glucopyranoside

Chemical Property:

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Technology Process of phenyl 2,3,4-tri-O-benzyl-6-O-[2-[(4-phenylbenzyl)oxycarbonyl]benzoyl]-1-thio-α-D-glucopyranoside

There total 1 articles about phenyl 2,3,4-tri-O-benzyl-6-O-[2-[(4-phenylbenzyl)oxycarbonyl]benzoyl]-1-thio-α-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

Phthalic acid mono-((2R,3R,4S,5R,6R)-3,4,5-tris-benzyloxy-6-phenylsulfanyl-tetrahydro-pyran-2-ylmethyl) ester + biphenyl-4-yl methanol (3597-91-9) → phenyl 2,3,4-tri-O-benzyl-6-O-[2-[(4-phenylbenzyl)oxycarbonyl]benzoyl]-1-thio-α-D-glucopyranoside (848866-41-1)

Guidance literature:

With dacarbazine; dmap; In dichloromethane;

DOI:10.1016/j.tetasy.2004.11.042

Reference yield: 83.0%

phenyl 2,3,4-tri-O-benzyl-6-O-[2-[(4-phenylbenzyl)oxycarbonyl]benzoyl]-1-thio-α-D-glucopyranoside (848866-41-1) + methyl 2,3,4-tri-O-benzyl-D-glucopyranoside (53008-65-4,641635-63-4) → methyl 2,3,4-tri-O-benzyl-6-O-[2-[(4-phenylbenzyl)oxycarbonyl]benzoyl]-α-D-glucopyranosyl-(1->6)-2,3,4-tri-O-benzyl-α-D-glucopyranoside

Guidance literature:

With trimethylsilyl trifluoromethanesulfonate; iodosylbenzene; In various solvent(s); at -20 ℃; for 0.75h;

DOI:10.1016/j.tetasy.2004.11.042

Reference yield: 75.0%

phenyl 2,3,4-tri-O-benzyl-6-O-[2-[(4-phenylbenzyl)oxycarbonyl]benzoyl]-1-thio-α-D-glucopyranoside (848866-41-1) + methyl O-2,3,6-tri-O-benzyl-α-D-glucopyranoside (19488-48-3) → methyl 2,3,4-tri-O-benzyl-6-O-[2-[(4-phenylbenzyl)oxycarbonyl]benzoyl]-α-D-glucopyranosyl-(1->4)-2,3,6-tri-O-benzyl-α-D-glucopyranoside

Guidance literature:

With trimethylsilyl trifluoromethanesulfonate; iodosylbenzene; In various solvent(s); at -20 ℃; for 6h;

DOI:10.1016/j.tetasy.2004.11.042

upstream raw materials:

biphenyl-4-yl methanol

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