((S)-1-(benzyloxy)-3-(octadecyloxy)propan-2-yl) 4-methylbenzenesulfonate

Base Information

Chemical Name:((S)-1-(benzyloxy)-3-(octadecyloxy)propan-2-yl) 4-methylbenzenesulfonate
CAS No.:83526-58-3
Molecular Formula:C₃₅H₅₆O₅S
Molecular Weight:588.893
Hs Code.:

Synonyms:((S)-1-(benzyloxy)-3-(octadecyloxy)propan-2-yl) 4-methylbenzenesulfonate

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Chemical Property of ((S)-1-(benzyloxy)-3-(octadecyloxy)propan-2-yl) 4-methylbenzenesulfonate

Chemical Property:

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Technology Process of ((S)-1-(benzyloxy)-3-(octadecyloxy)propan-2-yl) 4-methylbenzenesulfonate

There total 10 articles about ((S)-1-(benzyloxy)-3-(octadecyloxy)propan-2-yl) 4-methylbenzenesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 83526-57-2
(S)-1-(benzyloxy)-3-(octadecyloxy)propan-2-ol

: 98-59-9
p-toluenesulfonyl chloride

: 83526-58-3
((S)-1-(benzyloxy)-3-(octadecyloxy)propan-2-yl) 4-methylbenzenesulfonate

Guidance literature:: With pyridine; 1.) RT; 2.) 80 deg C, 4 h;
DOI:10.1002/hlca.19820650339

Reference yield:

: 83526-60-7
2-O-Acetyl-1-O-benzyl-3-O-octadecyl-sn-glycerin

: 83526-58-3
((S)-1-(benzyloxy)-3-(octadecyloxy)propan-2-yl) 4-methylbenzenesulfonate

Guidance literature:: Multi-step reaction with 6 steps

1: H₂ / 5percent Pd/C / tetrahydrofuran / Ambient temperature

2: phosphorus oxychloride, Et₃N, pyridine / CHCl₃ / Ambient temperature

3: 66 percent / LiAlH₄ / tetrahydrofuran / Ambient temperature

4: 71 percent / pyridine / CH₂Cl₂ / 48 h / Ambient temperature

5: toluene / 1 h / 80 °C

6: 100 percent / pyridine / 1.) RT; 2.) 80 deg C, 4 h

With pyridine; lithium aluminium tetrahydride; hydrogen; triethylamine; trichlorophosphate; palladium on activated charcoal; In tetrahydrofuran; dichloromethane; chloroform; toluene;
DOI:10.1002/hlca.19820650339

Reference yield:

: 3386-32-1
n-octadecyl p-toluenesulfonate

: 83526-58-3
((S)-1-(benzyloxy)-3-(octadecyloxy)propan-2-yl) 4-methylbenzenesulfonate

Guidance literature:: Multi-step reaction with 5 steps

1: 87 percent / NaH / dimethylformamide; petroleum ether / 3 h / 50 °C

2: 81.5 percent / 1N HCl / dioxane / 1 h / Heating

3: 71 percent / pyridine / CH₂Cl₂ / 48 h / Ambient temperature

4: toluene / 1 h / 80 °C

5: 100 percent / pyridine / 1.) RT; 2.) 80 deg C, 4 h

With pyridine; hydrogenchloride; sodium hydride; In 1,4-dioxane; dichloromethane; N,N-dimethyl-formamide; toluene; Petroleum ether;
DOI:10.1002/hlca.19820650339