O-(2,3,4-tri-O-benzyl-6-deoxy-α-D-xylo-hex-5-enopyranosyl)-(1->1)-2,3,4-tri-O-benzyl-6-deoxy-α-D-xylo-hex-5-enopyranoside

Base Information

Chemical Name:O-(2,3,4-tri-O-benzyl-6-deoxy-α-D-xylo-hex-5-enopyranosyl)-(1->1)-2,3,4-tri-O-benzyl-6-deoxy-α-D-xylo-hex-5-enopyranoside
CAS No.:221020-88-8
Molecular Formula:C₅₄H₅₄O₉
Molecular Weight:847.017
Hs Code.:

Synonyms:O-(2,3,4-tri-O-benzyl-6-deoxy-α-D-xylo-hex-5-enopyranosyl)-(1->1)-2,3,4-tri-O-benzyl-6-deoxy-α-D-xylo-hex-5-enopyranoside

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Chemical Property of O-(2,3,4-tri-O-benzyl-6-deoxy-α-D-xylo-hex-5-enopyranosyl)-(1->1)-2,3,4-tri-O-benzyl-6-deoxy-α-D-xylo-hex-5-enopyranoside

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Technology Process of O-(2,3,4-tri-O-benzyl-6-deoxy-α-D-xylo-hex-5-enopyranosyl)-(1->1)-2,3,4-tri-O-benzyl-6-deoxy-α-D-xylo-hex-5-enopyranoside

There total 2 articles about O-(2,3,4-tri-O-benzyl-6-deoxy-α-D-xylo-hex-5-enopyranosyl)-(1->1)-2,3,4-tri-O-benzyl-6-deoxy-α-D-xylo-hex-5-enopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 81105-73-9
2,2',3,3',4,4'-hexa-O-benzyl-6,6'-dideoxy-6,6'-diiodo-trehalose

: 221020-88-8
O-(2,3,4-tri-O-benzyl-6-deoxy-α-D-xylo-hex-5-enopyranosyl)-(1->1)-2,3,4-tri-O-benzyl-6-deoxy-α-D-xylo-hex-5-enopyranoside

Guidance literature:: With sodium hydride; In N,N-dimethyl-formamide; for 12h; 0 deg C to RT;
DOI:10.1016/S0040-4039(98)02662-8

Reference yield:

: 81105-71-7
2,3,4,2',3',4'-hexa-O-benzyl-6,6'-di-O-p-tolylsulfonyl-α,α-trehalose

: 221020-88-8
O-(2,3,4-tri-O-benzyl-6-deoxy-α-D-xylo-hex-5-enopyranosyl)-(1->1)-2,3,4-tri-O-benzyl-6-deoxy-α-D-xylo-hex-5-enopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: NaI / dimethylformamide

2: 96 percent / NaH / dimethylformamide / 12 h / 0 deg C to RT

With sodium hydride; sodium iodide; In N,N-dimethyl-formamide;
DOI:10.1016/S0040-4039(98)02662-8

Reference yield:

: 221020-88-8
O-(2,3,4-tri-O-benzyl-6-deoxy-α-D-xylo-hex-5-enopyranosyl)-(1->1)-2,3,4-tri-O-benzyl-6-deoxy-α-D-xylo-hex-5-enopyranoside

: [(2S,3R,4S,5R,6R)-3,4,5-Tris-benzyloxy-6-((2R,3R,4S,5R,6R)-3,4,5-tris-benzyloxy-6-hydroxymethyl-tetrahydro-pyran-2-yloxy)-tetrahydro-pyran-2-yl]-methanol

: 221020-89-9
O-(2,3,4-tri-O-benzyl-β-L-idopyranosyl)-(1->1)-2,3,4-tri-O-benzyl-β-L-idopyranoside

Guidance literature:: With dimethylsulfide borane complex; dihydrogen peroxide; Yield given; Multistep reaction. Yields of byproduct given; 1.) THF; 2.) THF;
DOI:10.1016/S0040-4039(98)02662-8