4-diisopropylaminooxalyl-N-(2-(R)-hydroxy-1-(S)-methyl-2-phenylethyl)-N-methylbenzamide

Base Information

Chemical Name:4-diisopropylaminooxalyl-N-(2-(R)-hydroxy-1-(S)-methyl-2-phenylethyl)-N-methylbenzamide
CAS No.:850013-10-4
Molecular Formula:C₂₅H₃₂N₂O₄
Molecular Weight:424.54
Hs Code.:

Synonyms:4-diisopropylaminooxalyl-N-(2-(R)-hydroxy-1-(S)-methyl-2-phenylethyl)-N-methylbenzamide

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Chemical Property of 4-diisopropylaminooxalyl-N-(2-(R)-hydroxy-1-(S)-methyl-2-phenylethyl)-N-methylbenzamide

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Technology Process of 4-diisopropylaminooxalyl-N-(2-(R)-hydroxy-1-(S)-methyl-2-phenylethyl)-N-methylbenzamide

There total 3 articles about 4-diisopropylaminooxalyl-N-(2-(R)-hydroxy-1-(S)-methyl-2-phenylethyl)-N-methylbenzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: N-[2-(tert-butyl-dimethyl-silanyloxy)-1-methyl-2-phenyl-ethyl]-4-diisopropylaminooxalyl-N-methyl-benzamide

: 850013-10-4
4-diisopropylaminooxalyl-N-(2-(R)-hydroxy-1-(S)-methyl-2-phenylethyl)-N-methylbenzamide

Guidance literature:: With tetrabutyl ammonium fluoride; In tetrahydrofuran;
DOI:10.1021/ja043999p

Reference yield:

: 299-42-3,7009-81-6,90-83-5,6912-63-6
ephedrine

: 850013-10-4
4-diisopropylaminooxalyl-N-(2-(R)-hydroxy-1-(S)-methyl-2-phenylethyl)-N-methylbenzamide

Guidance literature:: Multi-step reaction with 3 steps

1.1: 2,6-lutidine / CH₂Cl₂ / cooling

2.1: 1-[3-(dimethylamino)propyl]-3-ethylcarbodiimide*HCl / CH₂Cl₂ / 20 °C

2.2: CH₂Cl₂ / 20 °C

3.1: tetrabutylammonium fluoride / tetrahydrofuran

With 2,6-dimethylpyridine; tetrabutyl ammonium fluoride; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In tetrahydrofuran; dichloromethane;
DOI:10.1021/ja043999p

Reference yield:

: 130647-17-5
(1R,2S)-(-)-2-(methylamino)-1-phenyl-1<(tert-butyldimethylsilyl)oxy>-propane

: 850013-10-4
4-diisopropylaminooxalyl-N-(2-(R)-hydroxy-1-(S)-methyl-2-phenylethyl)-N-methylbenzamide

Guidance literature:: Multi-step reaction with 2 steps

1.1: 1-[3-(dimethylamino)propyl]-3-ethylcarbodiimide*HCl / CH₂Cl₂ / 20 °C

1.2: CH₂Cl₂ / 20 °C

2.1: tetrabutylammonium fluoride / tetrahydrofuran

With tetrabutyl ammonium fluoride; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In tetrahydrofuran; dichloromethane;
DOI:10.1021/ja043999p