C₁₇H₂₀O₄

Base Information

Chemical Name:C₁₇H₂₀O₄
CAS No.:1052083-49-4
Molecular Formula:C₁₇H₂₀O₄
Molecular Weight:288.343
Hs Code.:

C<sub>17</sub>H<sub>20</sub>O<sub>4</sub>

Synonyms:C₁₇H₂₀O₄

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Chemical Property of C₁₇H₂₀O₄

Chemical Property:

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Technology Process of C₁₇H₂₀O₄

There total 13 articles about C₁₇H₂₀O₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 1370368-76-5
C₁₇H₁₈O₄

: 1052083-49-4
C₁₇H₂₀O₄

Guidance literature:: With quinoline; Lindlar's catalyst; hydrogen; In methanol; ethyl acetate; at 20 ℃; for 6h;
DOI:10.1016/j.bmcl.2012.02.025

Reference yield:

: 1255639-74-7
C₂₂H₂₈O₂Si

: 1052083-49-4
C₁₇H₂₀O₄

Guidance literature:: Multi-step reaction with 11 steps

1: n-butyllithium / anhydride THF / 3 h / -20 °C

2: di-isopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran / 12 h / 0 - 20 °C

3: methanol; potassium carbonate / 1 h

4: tetrabutyl ammonium fluoride / tetrahydrofuran / 4 h / 0 - 20 °C

5: pyridinium p-toluenesulfonate / dichloromethane / 0.5 h / 0 °C

6: sodium periodate; osmium(VIII) oxide; 4-methylmorpholine N-oxide / water; acetone / 4 h / 27 °C

7: (R,R)-bis[iPrO-Ti(1,1'-binaphthyl-2,2'-diyldioxy)]O / dichloromethane / 72 h / -20 °C / Molecular sieve

8: N-ethyl-N,N-diisopropylamine / dichloromethane / 2 h / -78 °C

9: Grubbs catalyst first generation / dichloromethane / 12 h / Reflux

10: hydrogenchloride / methanol / 0.5 h / 0 °C

11: quinoline; Lindlar's catalyst; hydrogen / methanol; ethyl acetate / 6 h / 20 °C

With Grubbs catalyst first generation; quinoline; hydrogenchloride; methanol; sodium periodate; osmium(VIII) oxide; n-butyllithium; di-isopropyl azodicarboxylate; (R,R)-bis[iPrO-Ti(1,1'-binaphthyl-2,2'-diyldioxy)]O; Lindlar's catalyst; tetrabutyl ammonium fluoride; hydrogen; pyridinium p-toluenesulfonate; potassium carbonate; 4-methylmorpholine N-oxide; N-ethyl-N,N-diisopropylamine; triphenylphosphine; In tetrahydrofuran; methanol; anhydride THF; dichloromethane; water; ethyl acetate; acetone; 2: Mitsunobu reaction / 7: Maruoka asymmetric allylation;
DOI:10.1016/j.bmcl.2012.02.025

Reference yield:

: 1370368-72-1
C₂₉H₃₆O₂Si

: 1052083-49-4
C₁₇H₂₀O₄

Guidance literature:: Multi-step reaction with 11 steps

1: naphthalene; lithium / 3 h / -20 °C

2: 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione / dichloromethane; dimethyl sulfoxide / 6 h / 0 - 20 °C

3: n-butyllithium / anhydride THF / 3 h / -20 °C

4: tetrabutyl ammonium fluoride / tetrahydrofuran / 4 h / 0 - 20 °C

5: pyridinium p-toluenesulfonate / dichloromethane / 0.5 h / 0 °C

6: sodium periodate; osmium(VIII) oxide; 4-methylmorpholine N-oxide / water; acetone / 4 h / 27 °C

7: (R,R)-bis[iPrO-Ti(1,1'-binaphthyl-2,2'-diyldioxy)]O / dichloromethane / 72 h / -20 °C / Molecular sieve

8: N-ethyl-N,N-diisopropylamine / dichloromethane / 2 h / -78 °C

9: Grubbs catalyst first generation / dichloromethane / 12 h / Reflux

10: hydrogenchloride / methanol / 0.5 h / 0 °C

11: quinoline; Lindlar's catalyst; hydrogen / methanol; ethyl acetate / 6 h / 20 °C

With Grubbs catalyst first generation; quinoline; hydrogenchloride; sodium periodate; osmium(VIII) oxide; n-butyllithium; naphthalene; (R,R)-bis[iPrO-Ti(1,1'-binaphthyl-2,2'-diyldioxy)]O; Lindlar's catalyst; tetrabutyl ammonium fluoride; hydrogen; pyridinium p-toluenesulfonate; lithium; 4-methylmorpholine N-oxide; N-ethyl-N,N-diisopropylamine; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione; In tetrahydrofuran; methanol; anhydride THF; dichloromethane; water; dimethyl sulfoxide; ethyl acetate; acetone; 7: Maruoka asymmetric allylation;
DOI:10.1016/j.bmcl.2012.02.025