3,5-bis(3-{3,5-bis[3-(tert-butoxycarbonylamino)propoxy]benzamido}propoxy)benzyl methacrylate

Base Information

Chemical Name:3,5-bis(3-{3,5-bis[3-(tert-butoxycarbonylamino)propoxy]benzamido}propoxy)benzyl methacrylate
CAS No.:916264-94-3
Molecular Formula:C₆₃H₉₄N₆O₁₈
Molecular Weight:1223.47
Hs Code.:

Synonyms:3,5-bis(3-{3,5-bis[3-(tert-butoxycarbonylamino)propoxy]benzamido}propoxy)benzyl methacrylate

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Chemical Property of 3,5-bis(3-{3,5-bis[3-(tert-butoxycarbonylamino)propoxy]benzamido}propoxy)benzyl methacrylate

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Technology Process of 3,5-bis(3-{3,5-bis[3-(tert-butoxycarbonylamino)propoxy]benzamido}propoxy)benzyl methacrylate

There total 3 articles about 3,5-bis(3-{3,5-bis[3-(tert-butoxycarbonylamino)propoxy]benzamido}propoxy)benzyl methacrylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

: 3,5-bis(3-{3,5-bis[3-(tert-butoxycarbonylamino)propoxy]benzamido}propoxy)benzyl alcohol

: 920-46-7,26937-45-1
Methacryloyl chloride

: 916264-94-3
3,5-bis(3-{3,5-bis[3-(tert-butoxycarbonylamino)propoxy]benzamido}propoxy)benzyl methacrylate

Guidance literature:: With dmap; triethylamine; In N,N-dimethyl-formamide; at 20 ℃; for 16h;
DOI:10.1021/ja065113i

Reference yield:

: (3-{3-(3-tert-butoxycarbonylamino-propoxy)-5-[N-(3-dimethylamino-propyl)-N'-ethyl-carbamimidoyloxycarbonyl]-phenoxy}-propyl)-carbamic acid tert-butyl ester

: 916264-94-3
3,5-bis(3-{3,5-bis[3-(tert-butoxycarbonylamino)propoxy]benzamido}propoxy)benzyl methacrylate

Guidance literature:: Multi-step reaction with 2 steps

1: 10.4 g / triethylamine / CH₂Cl₂ / 16 h / 20 °C

2: 62 percent / triethylamine; 4-(dimethylamino)pyridine / dimethylformamide / 16 h / 20 °C

With dmap; triethylamine; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/ja065113i

Reference yield:

: 210355-20-7
3,5‐bis(3‐((tert‐butoxycarbonyl)amino)propoxy)benzoic acid

: 916264-94-3
3,5-bis(3-{3,5-bis[3-(tert-butoxycarbonylamino)propoxy]benzamido}propoxy)benzyl methacrylate

Guidance literature:: Multi-step reaction with 3 steps

1: N-hydroxybenzotriazole / CH₂Cl₂ / 4 h / -20 °C

2: 10.4 g / triethylamine / CH₂Cl₂ / 16 h / 20 °C

3: 62 percent / triethylamine; 4-(dimethylamino)pyridine / dimethylformamide / 16 h / 20 °C

With dmap; benzotriazol-1-ol; triethylamine; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/ja065113i