1-methyl-cis-3-phenylcyclobutyl tosylate

Base Information

Chemical Name:1-methyl-cis-3-phenylcyclobutyl tosylate
CAS No.:152714-16-4
Molecular Formula:C₁₈H₂₀O₃S
Molecular Weight:316.421
Hs Code.:

Synonyms:1-methyl-cis-3-phenylcyclobutyl tosylate

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Chemical Property of 1-methyl-cis-3-phenylcyclobutyl tosylate

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Technology Process of 1-methyl-cis-3-phenylcyclobutyl tosylate

There total 5 articles about 1-methyl-cis-3-phenylcyclobutyl tosylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 100-42-5,25038-60-2,25247-68-1,28213-80-1,28325-75-9,79637-11-9,9003-53-6
styrene

: 152714-16-4
1-methyl-cis-3-phenylcyclobutyl tosylate

Guidance literature:: Multi-step reaction with 6 steps

1: 62 percent / 43 h / 112 °C

2: 83 percent / KOH / aq. ethanol / 21 h / Ambient temperature

3: 78 percent / conc. H₂SO₄ / 0.28 h / Heating

4: 96 percent / AcONa, H₂ / Pd/C / methanol

5: 79 percent / diethyl ether / 2 h

6: 1.) n-BuLi / 1.) ether, hexane, 15 min, 2.) ether, hexane, 0 deg C, 5 h

With potassium hydroxide; n-butyllithium; sulfuric acid; hydrogen; sodium acetate; palladium on activated charcoal; In methanol; diethyl ether; ethanol;
DOI:10.1021/ja00076a024

Reference yield:

: 1716-70-7
2,2-dichloro-1,1-difluoro-3-phenyl-cyclobutane

: 152714-16-4
1-methyl-cis-3-phenylcyclobutyl tosylate

Guidance literature:: Multi-step reaction with 5 steps

1: 83 percent / KOH / aq. ethanol / 21 h / Ambient temperature

2: 78 percent / conc. H₂SO₄ / 0.28 h / Heating

3: 96 percent / AcONa, H₂ / Pd/C / methanol

4: 79 percent / diethyl ether / 2 h

5: 1.) n-BuLi / 1.) ether, hexane, 15 min, 2.) ether, hexane, 0 deg C, 5 h

With potassium hydroxide; n-butyllithium; sulfuric acid; hydrogen; sodium acetate; palladium on activated charcoal; In methanol; diethyl ether; ethanol;
DOI:10.1021/ja00076a024

Reference yield:

: 320-00-3
1,1-difluoro-2-chloro-3-phenyl-2-cyclobutene

: 152714-16-4
1-methyl-cis-3-phenylcyclobutyl tosylate

Guidance literature:: Multi-step reaction with 4 steps

1: 78 percent / conc. H₂SO₄ / 0.28 h / Heating

2: 96 percent / AcONa, H₂ / Pd/C / methanol

3: 79 percent / diethyl ether / 2 h

4: 1.) n-BuLi / 1.) ether, hexane, 15 min, 2.) ether, hexane, 0 deg C, 5 h

With n-butyllithium; sulfuric acid; hydrogen; sodium acetate; palladium on activated charcoal; In methanol; diethyl ether;
DOI:10.1021/ja00076a024