2-(trimethylsilyl)ethyl (methyl 4,7,8,9-tetra-O-acetyl-5-N,N-diacetylamino-3,5-dideoxy-3-phenylthio-D-erythro-β-L-gluco-non-2-ulopyranosylonate)-(2->3)-2-azido-6-O-benzoyl-2-deoxy-β-D-galactopyranoside

Base Information

Chemical Name:2-(trimethylsilyl)ethyl (methyl 4,7,8,9-tetra-O-acetyl-5-N,N-diacetylamino-3,5-dideoxy-3-phenylthio-D-erythro-β-L-gluco-non-2-ulopyranosylonate)-(2->3)-2-azido-6-O-benzoyl-2-deoxy-β-D-galactopyranoside
CAS No.:221524-14-7
Molecular Formula:C₄₆H₆₀N₄O₁₉SSi
Molecular Weight:1033.15
Hs Code.:

2-(trimethylsilyl)ethyl (methyl 4,7,8,9-tetra-O-acetyl-5-N,N-diacetylamino-3,5-dideoxy-3-phenylthio-D-erythro-β-L-gluco-non-2-ulopyranosylonate)-(2->3)-2-azido-6-O-benzoyl-2-deoxy-β-D-galactopyranoside

Synonyms:2-(trimethylsilyl)ethyl (methyl 4,7,8,9-tetra-O-acetyl-5-N,N-diacetylamino-3,5-dideoxy-3-phenylthio-D-erythro-β-L-gluco-non-2-ulopyranosylonate)-(2->3)-2-azido-6-O-benzoyl-2-deoxy-β-D-galactopyranoside

Suppliers and Price of 2-(trimethylsilyl)ethyl (methyl 4,7,8,9-tetra-O-acetyl-5-N,N-diacetylamino-3,5-dideoxy-3-phenylthio-D-erythro-β-L-gluco-non-2-ulopyranosylonate)-(2->3)-2-azido-6-O-benzoyl-2-deoxy-β-D-galactopyranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-(trimethylsilyl)ethyl (methyl 4,7,8,9-tetra-O-acetyl-5-N,N-diacetylamino-3,5-dideoxy-3-phenylthio-D-erythro-β-L-gluco-non-2-ulopyranosylonate)-(2->3)-2-azido-6-O-benzoyl-2-deoxy-β-D-galactopyranoside

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Technology Process of 2-(trimethylsilyl)ethyl (methyl 4,7,8,9-tetra-O-acetyl-5-N,N-diacetylamino-3,5-dideoxy-3-phenylthio-D-erythro-β-L-gluco-non-2-ulopyranosylonate)-(2->3)-2-azido-6-O-benzoyl-2-deoxy-β-D-galactopyranoside

There total 2 articles about 2-(trimethylsilyl)ethyl (methyl 4,7,8,9-tetra-O-acetyl-5-N,N-diacetylamino-3,5-dideoxy-3-phenylthio-D-erythro-β-L-gluco-non-2-ulopyranosylonate)-(2->3)-2-azido-6-O-benzoyl-2-deoxy-β-D-galactopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

: 151651-23-9
2-(trimethylsilyl)ethyl 2-azido-6-O-benzoyl-2-deoxy-β-D-galactopyranoside

: 221524-10-3
methyl onate

: 221524-14-7
2-(trimethylsilyl)ethyl (methyl 4,7,8,9-tetra-O-acetyl-5-N,N-diacetylamino-3,5-dideoxy-3-phenylthio-D-erythro-β-L-gluco-non-2-ulopyranosylonate)-(2->3)-2-azido-6-O-benzoyl-2-deoxy-β-D-galactopyranoside

Guidance literature:: With methanesulfonyl bromide; silver trifluoromethanesulfonate; In dichloromethane; acetonitrile; at -45 ℃;
DOI:10.1016/S0008-6215(02)00036-8

Reference yield:

: 156726-99-7
Methyl onate

: 221524-14-7
2-(trimethylsilyl)ethyl (methyl 4,7,8,9-tetra-O-acetyl-5-N,N-diacetylamino-3,5-dideoxy-3-phenylthio-D-erythro-β-L-gluco-non-2-ulopyranosylonate)-(2->3)-2-azido-6-O-benzoyl-2-deoxy-β-D-galactopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 97 percent / p-toluenesulfonic acid / 20 h / 60 °C

2: 66 percent / AgOTf; MeSBr / acetonitrile; CH₂Cl₂ / -45 °C

With methanesulfonyl bromide; silver trifluoromethanesulfonate; toluene-4-sulfonic acid; In dichloromethane; acetonitrile;
DOI:10.1016/S0008-6215(02)00036-8