Technology Process of C15H19FO5
There total 5 articles about C15H19FO5 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
sodium chlorite; sodium dihydrogenphosphate; 2-methyl-but-2-ene;
In
water; tert-butyl alcohol;
at 20 ℃;
DOI:10.3987/COM-08-11407
- Guidance literature:
-
Multi-step reaction with 4 steps
1: triethylsilane / dichloromethane / 20 °C
2: titanium(IV) tetraethanolate / 80 °C
3: titanium tetrachloride / dichloromethane / -78 - 20 °C
4: sodium dihydrogenphosphate; sodium chlorite; 2-methyl-but-2-ene / water; tert-butyl alcohol / 20 °C
With
triethylsilane; titanium(IV) tetraethanolate; sodium chlorite; sodium dihydrogenphosphate; 2-methyl-but-2-ene; titanium tetrachloride;
In
dichloromethane; water; tert-butyl alcohol;
4: Kraus oxidation;
DOI:10.3987/COM-08-11407
- Guidance literature:
-
Multi-step reaction with 3 steps
1: titanium(IV) tetraethanolate / 80 °C
2: titanium tetrachloride / dichloromethane / -78 - 20 °C
3: sodium dihydrogenphosphate; sodium chlorite; 2-methyl-but-2-ene / water; tert-butyl alcohol / 20 °C
With
titanium(IV) tetraethanolate; sodium chlorite; sodium dihydrogenphosphate; 2-methyl-but-2-ene; titanium tetrachloride;
In
dichloromethane; water; tert-butyl alcohol;
3: Kraus oxidation;
DOI:10.3987/COM-08-11407