(R)-1-[(2,4,6-triisopropylphenyl)sulfinyl]-2-naphthaldehyde dimethyl acetal

Base Information

Chemical Name:(R)-1-[(2,4,6-triisopropylphenyl)sulfinyl]-2-naphthaldehyde dimethyl acetal
CAS No.:320589-32-0
Molecular Formula:C₂₈H₃₆O₃S
Molecular Weight:452.658
Hs Code.:

Synonyms:(R)-1-[(2,4,6-triisopropylphenyl)sulfinyl]-2-naphthaldehyde dimethyl acetal

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Chemical Property of (R)-1-[(2,4,6-triisopropylphenyl)sulfinyl]-2-naphthaldehyde dimethyl acetal

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Technology Process of (R)-1-[(2,4,6-triisopropylphenyl)sulfinyl]-2-naphthaldehyde dimethyl acetal

There total 1 articles about (R)-1-[(2,4,6-triisopropylphenyl)sulfinyl]-2-naphthaldehyde dimethyl acetal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 103668-59-3
1-bromo-2-naphthaldehyde dimethyl acetal

: (R)-diacetone-D-glucosyl 2,4,6-triisopropylbenzenesulfinate

: 320589-32-0
(R)-1-[(2,4,6-triisopropylphenyl)sulfinyl]-2-naphthaldehyde dimethyl acetal

Guidance literature:: With n-butyllithium; In diethyl ether; at -105 ℃;
DOI:10.1021/jo005581p

Reference yield: 100.0%

: 320589-32-0
(R)-1-[(2,4,6-triisopropylphenyl)sulfinyl]-2-naphthaldehyde dimethyl acetal

: 289473-20-7
(R_S)-1-[(2,4,6-triisopropyl)sulfinyl]-2-naphthaldehyde

Guidance literature:: With sulfuric acid; silica gel; In dichloromethane; at 20 ℃; for 1h;
DOI:10.1021/jo005581p

Reference yield:

: 320589-32-0
(R)-1-[(2,4,6-triisopropylphenyl)sulfinyl]-2-naphthaldehyde dimethyl acetal

: 99412-45-0
(S)-naphthalen-2-yl(phenyl)methanol

Guidance literature:: Multi-step reaction with 3 steps

1: 100 percent / aq. H₂SO₄; SiO₂ / CH₂Cl₂ / 1 h / 20 °C

2: 96 percent / tetrahydrofuran / -78 °C

3: 61 percent / n-BuLi / tetrahydrofuran; hexane / 0.17 h / -78 °C

With n-butyllithium; sulfuric acid; silica gel; In tetrahydrofuran; hexane; dichloromethane;
DOI:10.1021/jo005581p