1-(2-nitrophenyl)-2-oxo-2-((9-oxo-9H-thioxanthen-2-yl)amino)ethyl 4-fluorobenzoate

Base Information

Chemical Name:1-(2-nitrophenyl)-2-oxo-2-((9-oxo-9H-thioxanthen-2-yl)amino)ethyl 4-fluorobenzoate
CAS No.:1622384-60-4
Molecular Formula:C₂₈H₁₇FN₂O₆S
Molecular Weight:528.517
Hs Code.:

Synonyms:1-(2-nitrophenyl)-2-oxo-2-((9-oxo-9H-thioxanthen-2-yl)amino)ethyl 4-fluorobenzoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-(2-nitrophenyl)-2-oxo-2-((9-oxo-9H-thioxanthen-2-yl)amino)ethyl 4-fluorobenzoate

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Technology Process of 1-(2-nitrophenyl)-2-oxo-2-((9-oxo-9H-thioxanthen-2-yl)amino)ethyl 4-fluorobenzoate

There total 2 articles about 1-(2-nitrophenyl)-2-oxo-2-((9-oxo-9H-thioxanthen-2-yl)amino)ethyl 4-fluorobenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 51.0%

: 456-22-4
4-Fluorobenzoic acid

: 1622384-59-1
2-isocyano-9H-thioxanthen-9-one

: 552-89-6
2-nitro-benzaldehyde

: 1622384-60-4
1-(2-nitrophenyl)-2-oxo-2-((9-oxo-9H-thioxanthen-2-yl)amino)ethyl 4-fluorobenzoate

Guidance literature:: In dichloromethane; for 20h; Solvent; Temperature; Reflux;
DOI:10.1002/anie.201402665

Reference yield:

: 33923-98-7
2-amino-9H-thioxanthen-9-one

: 1622384-60-4
1-(2-nitrophenyl)-2-oxo-2-((9-oxo-9H-thioxanthen-2-yl)amino)ethyl 4-fluorobenzoate

Guidance literature:: Multi-step reaction with 2 steps

1: sodium hydroxide; tetrabutylammomium bromide / dichloromethane; water / 1.25 h / 20 °C

2: dichloromethane / 20 h / Reflux

With tetrabutylammomium bromide; sodium hydroxide; In dichloromethane; water; 2: |Passerini Condensation;
DOI:10.1002/anie.201402665

Reference yield:

: 1622384-60-4
1-(2-nitrophenyl)-2-oxo-2-((9-oxo-9H-thioxanthen-2-yl)amino)ethyl 4-fluorobenzoate

: 456-22-4
4-Fluorobenzoic acid

Guidance literature:: With 2-(benzylamino)-1-(2-nitrophenyl)-2-oxoethyl 4-fluorobenzoate; In chloroform-d1; for 15h; Irradiation;
DOI:10.1002/anie.201402665