N-(3-chloro-2-formylphenyl)-4-methyl-N-(prop-2-yn-1-yl)benzenesulfonamide

Base Information

Chemical Name:N-(3-chloro-2-formylphenyl)-4-methyl-N-(prop-2-yn-1-yl)benzenesulfonamide
CAS No.:1439384-33-4
Molecular Formula:C₁₇H₁₄ClNO₃S
Molecular Weight:347.822
Hs Code.:

Synonyms:N-(3-chloro-2-formylphenyl)-4-methyl-N-(prop-2-yn-1-yl)benzenesulfonamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-(3-chloro-2-formylphenyl)-4-methyl-N-(prop-2-yn-1-yl)benzenesulfonamide

Chemical Property:

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Technology Process of N-(3-chloro-2-formylphenyl)-4-methyl-N-(prop-2-yn-1-yl)benzenesulfonamide

There total 1 articles about N-(3-chloro-2-formylphenyl)-4-methyl-N-(prop-2-yn-1-yl)benzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 46.0%

: N-(3-chloro-2-formylphenyl)-4-methylbenzenesulfonamide

: 106-96-7
propargyl bromide

: 1439384-33-4
N-(3-chloro-2-formylphenyl)-4-methyl-N-(prop-2-yn-1-yl)benzenesulfonamide

Guidance literature:: With potassium carbonate; In acetone; for 4h; Reflux;
DOI:10.1016/j.tet.2013.04.069

Reference yield:

: 1439384-33-4
N-(3-chloro-2-formylphenyl)-4-methyl-N-(prop-2-yn-1-yl)benzenesulfonamide

: 100-51-6,185532-71-2
benzyl alcohol

: C₂₄H₂₂ClNO₄S

Guidance literature:: With Echavarren's catalyst; In dichloromethane; at 20 ℃; for 2h; Inert atmosphere;
DOI:10.1016/j.tet.2013.04.069

Reference yield:

: 1439384-33-4
N-(3-chloro-2-formylphenyl)-4-methyl-N-(prop-2-yn-1-yl)benzenesulfonamide

: 1439383-98-8
6-chloro-1-tosyl-1H-benzo[b]azepin-3(2H)-one

Guidance literature:: Multi-step reaction with 2 steps

1: Echavarren's catalyst / dichloromethane / 2 h / 20 °C / Inert atmosphere

2: toluene-4-sulfonic acid / dichloromethane / 5 h / Reflux

With Echavarren's catalyst; toluene-4-sulfonic acid; In dichloromethane;
DOI:10.1016/j.tet.2013.04.069