C₃₆H₆₄O₇Si₂SO₂CH₂

Base Information

Chemical Name:C₃₆H₆₄O₇Si₂SO₂CH₂
CAS No.:945037-06-9
Molecular Formula:C₃₇H₆₆O₉SSi₂
Molecular Weight:743.163
Hs Code.:

C<sub>36</sub>H<sub>64</sub>O<sub>7</sub>Si<sub>2</sub>SO<sub>2</sub>CH<sub>2</sub>

Synonyms:C₃₆H₆₄O₇Si₂SO₂CH₂

Suppliers and Price of C₃₆H₆₄O₇Si₂SO₂CH₂

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of C₃₆H₆₄O₇Si₂SO₂CH₂

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of C₃₆H₆₄O₇Si₂SO₂CH₂

There total 10 articles about C₃₆H₆₄O₇Si₂SO₂CH₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 945036-98-6
C₇H₉Br₂OCH₃OSiC₆H₁₅SC₆H₅

: 945037-06-9
C₃₆H₆₄O₇Si₂SO₂CH₂

Guidance literature:: Multi-step reaction with 3 steps

1.1: n-butyllithium / tetrahydrofuran; hexane / 1 h / -78 °C

1.2: 75 percent / tetrahydrofuran; hexane / 5 h / -50 °C

2.1: 85 percent / H₂; quinoline / Pd/BaSO₄ / benzene / 10 h / 20 °C

3.1: 95 percent / pyridinium p-toluenesulfonate; molecular sieves 4 Angstroem / 10 h / 20 °C

With quinoline; n-butyllithium; 4 A molecular sieve; hydrogen; pyridinium p-toluenesulfonate; Pd-BaSO₄; In tetrahydrofuran; hexane; benzene;
DOI:10.1021/ol0707564

Reference yield:

: 945037-27-4
C₆H₅SC₂H₄CHOC₃H₅OCH₃C₆H₁₄Si

: 945037-06-9
C₃₆H₆₄O₇Si₂SO₂CH₂

Guidance literature:: Multi-step reaction with 6 steps

1.1: BH₂Cl / dioxane; CH₂Cl₂

1.2: NaOH; H₂O₂

2.1: PCC; molecular sieves 4 Angstroem / CH₂Cl₂ / 20 °C

3.1: 70 percent / PPh₃ / CH₂Cl₂ / 1 h / 0 °C

4.1: n-butyllithium / tetrahydrofuran; hexane / 1 h / -78 °C

4.2: 75 percent / tetrahydrofuran; hexane / 5 h / -50 °C

5.1: 85 percent / H₂; quinoline / Pd/BaSO₄ / benzene / 10 h / 20 °C

6.1: 95 percent / pyridinium p-toluenesulfonate; molecular sieves 4 Angstroem / 10 h / 20 °C

With quinoline; n-butyllithium; 4 A molecular sieve; hydrogen; pyridinium p-toluenesulfonate; chloroborane; triphenylphosphine; pyridinium chlorochromate; Pd-BaSO₄; In tetrahydrofuran; 1,4-dioxane; hexane; dichloromethane; benzene;
DOI:10.1021/ol0707564

Reference yield:

: 945037-26-3
C₆H₅SC₂H₄CHOC₃H₅OCH₃

: 945037-06-9
C₃₆H₆₄O₇Si₂SO₂CH₂

Guidance literature:: Multi-step reaction with 7 steps

1.1: 80 percent / imidazole / CH₂Cl₂

2.1: BH₂Cl / dioxane; CH₂Cl₂

2.2: NaOH; H₂O₂

3.1: PCC; molecular sieves 4 Angstroem / CH₂Cl₂ / 20 °C

4.1: 70 percent / PPh₃ / CH₂Cl₂ / 1 h / 0 °C

5.1: n-butyllithium / tetrahydrofuran; hexane / 1 h / -78 °C

5.2: 75 percent / tetrahydrofuran; hexane / 5 h / -50 °C

6.1: 85 percent / H₂; quinoline / Pd/BaSO₄ / benzene / 10 h / 20 °C

7.1: 95 percent / pyridinium p-toluenesulfonate; molecular sieves 4 Angstroem / 10 h / 20 °C

With 1H-imidazole; quinoline; n-butyllithium; 4 A molecular sieve; hydrogen; pyridinium p-toluenesulfonate; chloroborane; triphenylphosphine; pyridinium chlorochromate; Pd-BaSO₄; In tetrahydrofuran; 1,4-dioxane; hexane; dichloromethane; benzene;
DOI:10.1021/ol0707564