Technology Process of C23H25NO5
There total 3 articles about C23H25NO5 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
oxalyl dichloride; dimethyl sulfoxide; triethylamine;
In
dichloromethane;
at -78 - 20 ℃;
Inert atmosphere;
DOI:10.1021/jo1019927
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: potassium hexamethylsilazane / tetrahydrofuran; toluene / 0.5 h / -78 °C / Inert atmosphere
1.2: 2.75 h / -78 - 20 °C / Inert atmosphere
2.1: boron trifluoride diethyl etherate / toluene / 20 h / 0 - 20 °C / Inert atmosphere
3.1: oxalyl dichloride; dimethyl sulfoxide; triethylamine / dichloromethane / -78 - 20 °C / Inert atmosphere
With
oxalyl dichloride; boron trifluoride diethyl etherate; potassium hexamethylsilazane; dimethyl sulfoxide; triethylamine;
In
tetrahydrofuran; dichloromethane; toluene;
3.1: Swern oxidation;
DOI:10.1021/jo1019927
- Guidance literature:
-
Multi-step reaction with 2 steps
1: boron trifluoride diethyl etherate / toluene / 20 h / 0 - 20 °C / Inert atmosphere
2: oxalyl dichloride; dimethyl sulfoxide; triethylamine / dichloromethane / -78 - 20 °C / Inert atmosphere
With
oxalyl dichloride; boron trifluoride diethyl etherate; dimethyl sulfoxide; triethylamine;
In
dichloromethane; toluene;
2: Swern oxidation;
DOI:10.1021/jo1019927
