1,8-(N,N,N,N-tetra-tert-butoxycarbonyl)diamino-4-(N-benzyloxycarbonyl)-4-azooctane

Base Information

Chemical Name:1,8-(N,N,N,N-tetra-tert-butoxycarbonyl)diamino-4-(N-benzyloxycarbonyl)-4-azooctane
CAS No.:206347-06-0
Molecular Formula:C₃₅H₅₇N₃O₁₀
Molecular Weight:679.852
Hs Code.:

Synonyms:1,8-(N,N,N,N-tetra-tert-butoxycarbonyl)diamino-4-(N-benzyloxycarbonyl)-4-azooctane

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Chemical Property of 1,8-(N,N,N,N-tetra-tert-butoxycarbonyl)diamino-4-(N-benzyloxycarbonyl)-4-azooctane

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Technology Process of 1,8-(N,N,N,N-tetra-tert-butoxycarbonyl)diamino-4-(N-benzyloxycarbonyl)-4-azooctane

There total 4 articles about 1,8-(N,N,N,N-tetra-tert-butoxycarbonyl)diamino-4-(N-benzyloxycarbonyl)-4-azooctane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 24424-99-5
di-tert-butyl dicarbonate

: 113283-99-1
N⁴-benzyloxycarbonyl-N¹,N⁸-di-tert-butoxycarbonylspermidine

: 206347-06-0
1,8-(N,N,N,N-tetra-tert-butoxycarbonyl)diamino-4-(N-benzyloxycarbonyl)-4-azooctane

Guidance literature:: With dmap; In acetonitrile; for 6h; Ambient temperature;
DOI:10.1016/S0040-4020(98)00114-8

Reference yield:

: 124-20-9
N-(3-aminopropyl)-1,4-diaminobutane

: 206347-06-0
1,8-(N,N,N,N-tetra-tert-butoxycarbonyl)diamino-4-(N-benzyloxycarbonyl)-4-azooctane

Guidance literature:: Multi-step reaction with 3 steps

1: tetrahydrofuran / Ambient temperature

2: 88 percent / 2M Na₂CO₃, 2M NaOH / dioxane / 16 h / 4 °C

3: 74 percent / DMAP / acetonitrile / 6 h / Ambient temperature

With dmap; sodium hydroxide; sodium carbonate; In tetrahydrofuran; 1,4-dioxane; acetonitrile;
DOI:10.1016/S0040-4020(98)00114-8

Reference yield:

: 58632-95-4
2-(tert-Butoxycarbonyloxyimino)-2-phenylacetonitrile

: 206347-06-0
1,8-(N,N,N,N-tetra-tert-butoxycarbonyl)diamino-4-(N-benzyloxycarbonyl)-4-azooctane

Guidance literature:: Multi-step reaction with 3 steps

1: tetrahydrofuran / Ambient temperature

2: 88 percent / 2M Na₂CO₃, 2M NaOH / dioxane / 16 h / 4 °C

3: 74 percent / DMAP / acetonitrile / 6 h / Ambient temperature

With dmap; sodium hydroxide; sodium carbonate; In tetrahydrofuran; 1,4-dioxane; acetonitrile;
DOI:10.1016/S0040-4020(98)00114-8