2,5-Bis-(4-chloro-phenylamino)-3,6-dioxo-cyclohexa-1,4-dienecarboxylic acid ethyl ester

Base Information

Chemical Name:2,5-Bis-(4-chloro-phenylamino)-3,6-dioxo-cyclohexa-1,4-dienecarboxylic acid ethyl ester
CAS No.:137058-32-3
Molecular Formula:C₂₁H₁₆Cl₂N₂O₄
Molecular Weight:431.275
Hs Code.:

Synonyms:2,5-Bis-(4-chloro-phenylamino)-3,6-dioxo-cyclohexa-1,4-dienecarboxylic acid ethyl ester

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Chemical Property of 2,5-Bis-(4-chloro-phenylamino)-3,6-dioxo-cyclohexa-1,4-dienecarboxylic acid ethyl ester

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Technology Process of 2,5-Bis-(4-chloro-phenylamino)-3,6-dioxo-cyclohexa-1,4-dienecarboxylic acid ethyl ester

There total 1 articles about 2,5-Bis-(4-chloro-phenylamino)-3,6-dioxo-cyclohexa-1,4-dienecarboxylic acid ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 3943-91-7
ethyl 2,5-dihydroxybenzoate

: 106-47-8
4-chloro-aniline

: 137058-32-3
2,5-Bis-(4-chloro-phenylamino)-3,6-dioxo-cyclohexa-1,4-dienecarboxylic acid ethyl ester

Guidance literature:: With sodium periodate; In methanol; water; at 0 - 20 ℃; for 19h;
DOI:10.1021/jm00115a019

Reference yield: 88.0%

: 137058-32-3
2,5-Bis-(4-chloro-phenylamino)-3,6-dioxo-cyclohexa-1,4-dienecarboxylic acid ethyl ester

: 137058-36-7
2-Amino-5-(4-chloro-phenylamino)-3,6-dioxo-cyclohexa-1,4-dienecarboxylic acid ethyl ester

Guidance literature:: With ammonia; In methanol; chloroform; for 18h; Ambient temperature;
DOI:10.1021/jm00115a019

Reference yield:

: 137058-32-3
2,5-Bis-(4-chloro-phenylamino)-3,6-dioxo-cyclohexa-1,4-dienecarboxylic acid ethyl ester

: 137058-53-8
5-(4-Chloro-phenylamino)-3-(2-piperidin-1-yl-ethylamino)-benzo[c]isoxazole-4,7-dione

Guidance literature:: Multi-step reaction with 3 steps

1: 88 percent / NH₃ / CHCl₃; methanol / 18 h / Ambient temperature

2: 55 percent / Pd(OAc)4 / CHCl₃; tetrahydrofuran / 1.5 h

3: 38 percent / ethanol / 3 h / Ambient temperature

With palladium(II) acetate; ammonia; In tetrahydrofuran; methanol; ethanol; chloroform;
DOI:10.1021/jm00115a019