C₂₄H₂₃N₃O₄

Base Information

Chemical Name:C₂₄H₂₃N₃O₄
CAS No.:1177423-33-4
Molecular Formula:C₂₄H₂₃N₃O₄
Molecular Weight:417.464
Hs Code.:

C<sub>24</sub>H<sub>23</sub>N<sub>3</sub>O<sub>4</sub>

Synonyms:C₂₄H₂₃N₃O₄

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Chemical Property of C₂₄H₂₃N₃O₄

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Technology Process of C₂₄H₂₃N₃O₄

There total 11 articles about C₂₄H₂₃N₃O₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 2C₂HF₃O₂*C₂₅H₂₅N₃O₄

: 1177423-33-4
C₂₄H₂₃N₃O₄

Guidance literature:: 2C₂HF₃O₂*C₂₅H₂₅N₃O₄; With sodium isopropanethiolate; In N,N-dimethyl-formamide; at 50 ℃; for 1h;

With hydrogenchloride; water; In N,N-dimethyl-formamide;

Reference yield:

: 1177423-29-8
C₂₄H₂₂N₂O₅

: 1177423-33-4
C₂₄H₂₃N₃O₄

Guidance literature:: Multi-step reaction with 3 steps

1.1: water; sodium hydroxide / tetrahydrofuran; methanol; dichloromethane / 4 h / 20 °C

2.1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 0.5 h / 20 °C

2.2: 24 h

3.1: sodium isopropanethiolate / N,N-dimethyl-formamide / 1 h / 50 °C

With water; sodium isopropanethiolate; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; sodium hydroxide; In tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide;

Reference yield:

: 88912-27-0
3-chloro-isonicotinic acid

: 1177423-33-4
C₂₄H₂₃N₃O₄

Guidance literature:: Multi-step reaction with 9 steps

1.1: potassium carbonate / dimethyl sulfoxide / 0.5 h

1.2: 2 h / 20 °C

2.1: n-butyllithium; diisopropylamine / tetrahydrofuran; hexane / 1 h / -78 °C

2.2: 1 h / -78 °C

3.1: acetic acid / N,N-dimethyl-formamide / 62 h / 140 °C

4.1: sodium tetrahydroborate / methanol; dichloromethane / 3 h / 0 °C

5.1: dmap / dichloromethane / 0 - 20 °C

6.1: titanium tetrachloride / dichloromethane / 0.08 h / 0 °C

6.2: 1 h / 0 °C

7.1: water; sodium hydroxide / tetrahydrofuran; methanol; dichloromethane / 4 h / 20 °C

8.1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 0.5 h / 20 °C

8.2: 24 h

9.1: sodium isopropanethiolate / N,N-dimethyl-formamide / 1 h / 50 °C

With dmap; sodium tetrahydroborate; n-butyllithium; water; sodium isopropanethiolate; titanium tetrachloride; potassium carbonate; benzotriazol-1-ol; acetic acid; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; diisopropylamine; N-ethyl-N,N-diisopropylamine; sodium hydroxide; In tetrahydrofuran; methanol; hexane; dichloromethane; dimethyl sulfoxide; N,N-dimethyl-formamide;