C₃₂H₄₂O₅Si

Base Information

Chemical Name:C₃₂H₄₂O₅Si
CAS No.:1261152-44-6
Molecular Formula:C₃₂H₄₂O₅Si
Molecular Weight:534.768
Hs Code.:

C<sub>32</sub>H<sub>42</sub>O<sub>5</sub>Si

Synonyms:C₃₂H₄₂O₅Si

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Chemical Property of C₃₂H₄₂O₅Si

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Technology Process of C₃₂H₄₂O₅Si

There total 1 articles about C₃₂H₄₂O₅Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 1261152-28-6
C₃₉H₄₆O₅Si

: 1261152-44-6
C₃₂H₄₂O₅Si

Guidance literature:: With 10-camphorsufonic acid; In tetrahydrofuran; methanol; at 25 ℃; for 2h; Inert atmosphere;
DOI:10.1021/ja109533y

Reference yield: 98.0%

: 1261152-44-6
C₃₂H₄₂O₅Si

: 69739-34-0
t-butyldimethylsiyl triflate

: 1261152-45-7
C₄₄H₇₀O₅Si₃

Guidance literature:: With 2,6-dimethylpyridine; In dichloromethane; at 25 ℃; for 2h; Inert atmosphere;
DOI:10.1021/ja109533y

Reference yield:

: 1261152-44-6
C₃₂H₄₂O₅Si

: 1261152-35-5
C₇₀H₉₈O₉Si₃

Guidance literature:: Multi-step reaction with 18 steps

1.1: 2,6-dimethylpyridine / dichloromethane / 2 h / 25 °C / Inert atmosphere

2.1: 10-camphorsufonic acid / methanol / 3 h / 25 °C / Inert atmosphere

3.1: tetrapropylammonium perruthennate; 4-methylmorpholine N-oxide / dichloromethane / 0 - 25 °C / Inert atmosphere; Molecular sieve

4.1: sodium hexamethyldisilazane / tetrahydrofuran; toluene / 0.5 h / 0 °C / Inert atmosphere

4.2: -78 - 0 °C / Inert atmosphere

5.1: p-toluenesulfonic acid monohydrate / methanol; dichloromethane / 3 h / 25 °C / Inert atmosphere

6.1: 1H-imidazole / dichloromethane / 1 h / 25 °C / Inert atmosphere

7.1: bis(cyclohexanyl)borane / tetrahydrofuran / 0 - 25 °C / Inert atmosphere

7.2: 1 h / 0 °C / Inert atmosphere

8.1: sodium hydrogencarbonate; Dess-Martin periodane / dichloromethane / 3 h / 25 °C / Inert atmosphere

9.1: sodium dihydrogenphosphate; sodium chlorite; 2-methyl-but-2-ene / water; tert-butyl alcohol / 0.5 h / 25 °C / Inert atmosphere

10.1: dmap; 2-methyl-6-nitrobenzoic anhydride; triethylamine / toluene / 0.33 h / 25 °C / Inert atmosphere; Molecular sieve

10.2: 13 h / 25 °C / Inert atmosphere; Molecular sieve

11.1: p-toluenesulfonic acid monohydrate / methanol; dichloromethane / 0.67 h / 0 °C / Inert atmosphere

12.1: N,N,N,N,-tetramethylethylenediamine; titanium tetrachloride / tetrahydrofuran; dichloromethane / 0 - 25 °C / Inert atmosphere

12.2: 0.67 h / 25 °C / Inert atmosphere

13.1: 2,6-dimethylpyridine / dichloromethane / 1 h / 0 °C / Inert atmosphere

14.1: bis(cyclohexanyl)borane / tetrahydrofuran / 6 h / 25 °C / Inert atmosphere

14.2: 20 h / 0 °C / Inert atmosphere

15.1: sodium hydrogencarbonate; Dess-Martin periodane / dichloromethane / 0 - 25 °C / Inert atmosphere

16.1: p-toluenesulfonic acid monohydrate / methanol; dichloromethane / 0.5 h / 0 °C / Inert atmosphere

17.1: zinc trifluoromethanesulfonate / dichloromethane / 16 h / 25 °C / Inert atmosphere

18.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / -78 - 30 °C / Inert atmosphere

18.2: -78 - 0 °C / Inert atmosphere

With 1H-imidazole; 2,6-dimethylpyridine; dmap; sodium chlorite; sodium dihydrogenphosphate; tetrapropylammonium perruthennate; 2-methyl-but-2-ene; N,N,N,N,-tetramethylethylenediamine; bis(cyclohexanyl)borane; 10-camphorsufonic acid; 2-methyl-6-nitrobenzoic anhydride; p-toluenesulfonic acid monohydrate; sodium hexamethyldisilazane; titanium tetrachloride; zinc trifluoromethanesulfonate; sodium hydrogencarbonate; Dess-Martin periodane; 4-methylmorpholine N-oxide; triethylamine; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; methanol; dichloromethane; water; toluene; tert-butyl alcohol; 4.1: Wittig reaction / 4.2: Wittig reaction / 7.1: Hydroboration reaction / 14.1: Hydroboration reaction;
DOI:10.1021/ja109533y