(2S,3S)-3-Ethyl-2-[(S)-((R)-2-oxo-1,2-diphenyl-ethoxy)-phenyl-methyl]-cyclohexanone

Base Information

Chemical Name:(2S,3S)-3-Ethyl-2-[(S)-((R)-2-oxo-1,2-diphenyl-ethoxy)-phenyl-methyl]-cyclohexanone
CAS No.:347144-07-4
Molecular Formula:C₂₉H₃₀O₃
Molecular Weight:426.555
Hs Code.:

Synonyms:(2S,3S)-3-Ethyl-2-[(S)-((R)-2-oxo-1,2-diphenyl-ethoxy)-phenyl-methyl]-cyclohexanone

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Chemical Property of (2S,3S)-3-Ethyl-2-[(S)-((R)-2-oxo-1,2-diphenyl-ethoxy)-phenyl-methyl]-cyclohexanone

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Technology Process of (2S,3S)-3-Ethyl-2-[(S)-((R)-2-oxo-1,2-diphenyl-ethoxy)-phenyl-methyl]-cyclohexanone

There total 4 articles about (2S,3S)-3-Ethyl-2-[(S)-((R)-2-oxo-1,2-diphenyl-ethoxy)-phenyl-methyl]-cyclohexanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 347144-04-1
(2S,3S)-3-Ethyl-2-[(S)-((1R,2R)-2-hydroxy-1,2-diphenyl-ethoxy)-phenyl-methyl]-cyclohexanone

: 347144-07-4
(2S,3S)-3-Ethyl-2-[(S)-((R)-2-oxo-1,2-diphenyl-ethoxy)-phenyl-methyl]-cyclohexanone

Guidance literature:: With dipyridinium dichromate; 3 A molecular sieve; In dichloromethane; at 20 ℃; for 36h;
DOI:10.1021/ja005911n

Reference yield:

: 213987-19-0
(4R,5R)-2,4,5-triphenyl-1,3-dioxolane

: 347144-07-4
(2S,3S)-3-Ethyl-2-[(S)-((R)-2-oxo-1,2-diphenyl-ethoxy)-phenyl-methyl]-cyclohexanone

Guidance literature:: Multi-step reaction with 3 steps

1: CH₂Cl₂; hexane / 0 °C

2: 344 mg / Amberlyst-15 / methanol / 20 °C

3: 94 percent / PDC; 3 Angstroem molecular sieves / CH₂Cl₂ / 36 h / 20 °C

With dipyridinium dichromate; amberlyst-15; 3 A molecular sieve; In methanol; hexane; dichloromethane;
DOI:10.1021/ja005911n

Reference yield:

: C₁₀H₁₈OZn

: 347144-07-4
(2S,3S)-3-Ethyl-2-[(S)-((R)-2-oxo-1,2-diphenyl-ethoxy)-phenyl-methyl]-cyclohexanone

Guidance literature:: Multi-step reaction with 3 steps

1: CH₂Cl₂; hexane / 0 °C

2: 344 mg / Amberlyst-15 / methanol / 20 °C

3: 94 percent / PDC; 3 Angstroem molecular sieves / CH₂Cl₂ / 36 h / 20 °C

With dipyridinium dichromate; amberlyst-15; 3 A molecular sieve; In methanol; hexane; dichloromethane;
DOI:10.1021/ja005911n