2,4,5-trifluorobenzene magnesium chloride

Base Information

Chemical Name:2,4,5-trifluorobenzene magnesium chloride
CAS No.:1352613-28-5
Molecular Formula:C₆H₂ClF₃Mg
Molecular Weight:190.835
Hs Code.:

Synonyms:2,4,5-trifluorobenzene magnesium chloride

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Chemical Property of 2,4,5-trifluorobenzene magnesium chloride

Chemical Property:

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Technology Process of 2,4,5-trifluorobenzene magnesium chloride

There total 1 articles about 2,4,5-trifluorobenzene magnesium chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 367-23-7
1,2,4-trifluorobenzene

: 1068-55-9
isopropylmagnesium chloride

: 1352613-28-5
2,4,5-trifluorobenzene magnesium chloride

Guidance literature:: In tetrahydrofuran; at -20 - 10 ℃; for 3h; Product distribution / selectivity;

Reference yield: 93.0%

: 1117-71-1,56699-18-4,6000-00-6
methyl-4-bromo-2-butenoate

: 1352613-28-5
2,4,5-trifluorobenzene magnesium chloride

: 1260029-44-4
(E)-4-(2,4,5-trifluoro-phenyl)-but-2-enoic acid methyl ester

Guidance literature:: N,N,N,N,-tetramethylethylenediamine; cobalt(II) bromide; In tetrahydrofuran; at -20 - 0 ℃; Inert atmosphere;

Reference yield:

: 1352613-28-5
2,4,5-trifluorobenzene magnesium chloride

: 1369995-39-0
methyl 3-benzylamino-4-(2,4,5-trifluorophenyl)butanoate

Guidance literature:: Multi-step reaction with 3 steps

1.1: cobalt(II) bromide / N,N,N,N,-tetramethylethylenediamine / tetrahydrofuran / 0.5 h / 0 °C

1.2: 16 h / -20 - 0 °C

2.1: copper(II) carbonate / triphenylphosphine / water / 24.5 h / 20 °C / Inert atmosphere

3.1: boron trichloride / toluene / 20 °C / Inert atmosphere

3.2: 20 °C / Cooling with ice

With copper(II) carbonate; boron trichloride; cobalt(II) bromide; N,N,N,N,-tetramethylethylenediamine; triphenylphosphine; In tetrahydrofuran; water; toluene;