(Z)-phenylmethyl <2-<4-<(2,4-dioxo-5-thiazolidinylidene)methyl>phenoxy>ethyl>methylcarbamate

Base Information

Chemical Name:(Z)-phenylmethyl <2-<4-<(2,4-dioxo-5-thiazolidinylidene)methyl>phenoxy>ethyl>methylcarbamate
CAS No.:901120-42-1
Molecular Formula:C₂₁H₂₀N₂O₅S
Molecular Weight:412.466
Hs Code.:

Synonyms:(Z)-phenylmethyl <2-<4-<(2,4-dioxo-5-thiazolidinylidene)methyl>phenoxy>ethyl>methylcarbamate

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Chemical Property of (Z)-phenylmethyl <2-<4-<(2,4-dioxo-5-thiazolidinylidene)methyl>phenoxy>ethyl>methylcarbamate

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Technology Process of (Z)-phenylmethyl <2-<4-<(2,4-dioxo-5-thiazolidinylidene)methyl>phenoxy>ethyl>methylcarbamate

There total 5 articles about (Z)-phenylmethyl <2-<4-<(2,4-dioxo-5-thiazolidinylidene)methyl>phenoxy>ethyl>methylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 2295-31-0
thiazoline-2,4-dione

: 142649-87-4
phenylmethyl <2-(4-formylphenoxy)ethyl>methylcarbamate

: 901120-42-1
(Z)-phenylmethyl <2-<4-<(2,4-dioxo-5-thiazolidinylidene)methyl>phenoxy>ethyl>methylcarbamate

Guidance literature:: With piperidine; In ethanol; toluene; for 22h; Heating;
DOI:10.1039/b600848h

Reference yield:

: 67580-96-5
benzyl (2-hydroxyethyl)methylcarbamate

: 901120-42-1
(Z)-phenylmethyl <2-<4-<(2,4-dioxo-5-thiazolidinylidene)methyl>phenoxy>ethyl>methylcarbamate

Guidance literature:: Multi-step reaction with 2 steps

1: 80 percent / PPh₃; DEAD / tetrahydrofuran / 24 h / 20 °C

2: 84 percent / piperidine / ethanol; toluene / 22 h / Heating

With piperidine; triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; ethanol; toluene; 1: Mitsunobu reaction / 2: Knoevenagel condensation;
DOI:10.1039/b600848h

Reference yield:

: 123-08-0,65581-83-1
4-hydroxy-benzaldehyde

: 901120-42-1
(Z)-phenylmethyl <2-<4-<(2,4-dioxo-5-thiazolidinylidene)methyl>phenoxy>ethyl>methylcarbamate

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) NaH / 1.) DMF, RT, 1 h, 2.) DMF, 80 deg C, 18 h

2: 83 percent / piperidinium benzoate / toluene / 5 h / Heating

With piperidinium benzoate; sodium hydride; In toluene;
DOI:10.1021/jm00049a017