E-3-(3,4-dimethoxyphenyl)-N-(3,5,5,8,8-pentamethyl-5,6,7,8-tetrahydronaphthalen-2-yl)acrylamide

Base Information

Chemical Name:E-3-(3,4-dimethoxyphenyl)-N-(3,5,5,8,8-pentamethyl-5,6,7,8-tetrahydronaphthalen-2-yl)acrylamide
CAS No.:1271910-84-9
Molecular Formula:C₂₆H₃₃NO₃
Molecular Weight:407.553
Hs Code.:

Synonyms:E-3-(3,4-dimethoxyphenyl)-N-(3,5,5,8,8-pentamethyl-5,6,7,8-tetrahydronaphthalen-2-yl)acrylamide

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Chemical Property of E-3-(3,4-dimethoxyphenyl)-N-(3,5,5,8,8-pentamethyl-5,6,7,8-tetrahydronaphthalen-2-yl)acrylamide

Chemical Property:

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Technology Process of E-3-(3,4-dimethoxyphenyl)-N-(3,5,5,8,8-pentamethyl-5,6,7,8-tetrahydronaphthalen-2-yl)acrylamide

There total 6 articles about E-3-(3,4-dimethoxyphenyl)-N-(3,5,5,8,8-pentamethyl-5,6,7,8-tetrahydronaphthalen-2-yl)acrylamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 39856-08-1,141236-46-6
(E)-3,4-dimethoxycinnamic chloride

: 116233-17-1
3-methyl-5,6,7,8-tetrahydro-5,5,8,8-tetramethyl-2-naphthylamine

: 1271910-84-9
E-3-(3,4-dimethoxyphenyl)-N-(3,5,5,8,8-pentamethyl-5,6,7,8-tetrahydronaphthalen-2-yl)acrylamide

Guidance literature:: With triethylamine; In benzene; at -5 ℃; for 4h; Reflux;
DOI:10.1016/j.ejmech.2010.11.021

Reference yield:

: 6223-78-5
2,5-dichloro-2,5-dimethyl hexane

: 1271910-84-9
E-3-(3,4-dimethoxyphenyl)-N-(3,5,5,8,8-pentamethyl-5,6,7,8-tetrahydronaphthalen-2-yl)acrylamide

Guidance literature:: Multi-step reaction with 4 steps

1: aluminum (III) chloride

2: sulfuric acid; nitric acid / -10 °C

3: 10% palladium on activated carbon; hydrogen / ethanol / 1810.07 Torr

4: triethylamine / benzene / 4 h / -5 °C / Reflux

With aluminum (III) chloride; sulfuric acid; 10% palladium on activated carbon; hydrogen; nitric acid; triethylamine; In ethanol; benzene;
DOI:10.1016/j.ejmech.2010.11.021

Reference yield:

: 14737-89-4
3,4-dimethoxy-trans-cinnamic acid

: 1271910-84-9
E-3-(3,4-dimethoxyphenyl)-N-(3,5,5,8,8-pentamethyl-5,6,7,8-tetrahydronaphthalen-2-yl)acrylamide

Guidance literature:: Multi-step reaction with 2 steps

1: thionyl chloride / benzene / 5 h / Reflux

2: triethylamine / benzene / 4 h / -5 °C / Reflux

With thionyl chloride; triethylamine; In benzene;
DOI:10.1016/j.ejmech.2010.11.021