sulfure de p-methoxybenzyle et de pentene-4 yle-1

Base Information

Chemical Name:sulfure de p-methoxybenzyle et de pentene-4 yle-1
CAS No.:82944-29-4
Molecular Formula:C₁₃H₁₈OS
Molecular Weight:222.351
Hs Code.:

Synonyms:sulfure de p-methoxybenzyle et de pentene-4 yle-1

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Chemical Property of sulfure de p-methoxybenzyle et de pentene-4 yle-1

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Technology Process of sulfure de p-methoxybenzyle et de pentene-4 yle-1

There total 1 articles about sulfure de p-methoxybenzyle et de pentene-4 yle-1 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 6258-60-2
p-methoxybenzylmercaptan

: 1119-51-3
bromopentene

: 82944-29-4
sulfure de p-methoxybenzyle et de pentene-4 yle-1

Guidance literature:: With sodium hydroxide; In water; for 3h; Heating;

Reference yield: 87.0%

: 82944-29-4
sulfure de p-methoxybenzyle et de pentene-4 yle-1

: 19226-36-9
3-phenyl-5H-1,4,2-dioxazol-5-one

: N-(1-((4-methoxybenzyl)thio)pentan-3-yl)benzamide

Guidance literature:: With nickel(II) perchlorate hexahydrate; 2,9-di-n-butyl-1,10-phenanthroline; 4,4,5,5-tetramethyl-[1,3,2]-dioxaboralane; In tetrahydrofuran; at 20 ℃; for 3h; regioselective reaction; Inert atmosphere; Sealed tube;
DOI:10.1021/jacs.1c05834

Reference yield: 61.0%

: 82944-29-4
sulfure de p-methoxybenzyle et de pentene-4 yle-1

: 19226-36-9
3-phenyl-5H-1,4,2-dioxazol-5-one

: N-(5-((4-methoxybenzyl)thio)pentan-2-yl)benzamide

: N-(1-((4-methoxybenzyl)thio)pentan-3-yl)benzamide

Guidance literature:: With 2-methyl-1,10-phenanthroline; nickel(II) perchlorate hexahydrate; 4,4,5,5-tetramethyl-[1,3,2]-dioxaboralane; In tetrahydrofuran; at 20 ℃; for 3h; regioselective reaction; Inert atmosphere; Sealed tube;
DOI:10.1021/jacs.1c05834