C₂₃H₃₈O₅Si

Base Information

Chemical Name:C₂₃H₃₈O₅Si
CAS No.:1592771-10-2
Molecular Formula:C₂₃H₃₈O₅Si
Molecular Weight:422.637
Hs Code.:

C<sub>23</sub>H<sub>38</sub>O<sub>5</sub>Si

Synonyms:C₂₃H₃₈O₅Si

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Chemical Property of C₂₃H₃₈O₅Si

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Technology Process of C₂₃H₃₈O₅Si

There total 12 articles about C₂₃H₃₈O₅Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 1592771-62-4
C₂₃H₃₈O₅Si

: 1592771-10-2
C₂₃H₃₈O₅Si

Guidance literature:: With potassium hexamethylsilazane; In tetrahydrofuran; toluene; at 0 ℃; for 0.5h; diastereoselective reaction; Inert atmosphere;
DOI:10.1021/ol500788c

Reference yield:

: methyl 3-O-benzyl-5-O-(p-toluenesulfonyl)-2-deoxy-D-ribofuranoside

: 1592771-10-2
C₂₃H₃₈O₅Si

Guidance literature:: Multi-step reaction with 6 steps

1: lithium triethylborohydride / tetrahydrofuran / 6.25 h / 20 - 45 °C / Inert atmosphere

2: boron trifluoride diethyl etherate / dichloromethane / 0.67 h / 0 - 20 °C / Inert atmosphere

3: 4-methyl-morpholine / dichloromethane / 2 h / 20 °C / Inert atmosphere

4: methyl iodide; sodium hydrogencarbonate / acetonitrile; water / 24 h / 20 °C

5: samarium diiodide / acetonitrile; methanol / 1 h / -20 °C / Inert atmosphere

6: 2,6-dimethylpyridine / dichloromethane / 0.75 h / 0 - 20 °C / Inert atmosphere

With 4-methyl-morpholine; 2,6-dimethylpyridine; samarium diiodide; boron trifluoride diethyl etherate; lithium triethylborohydride; sodium hydrogencarbonate; methyl iodide; In tetrahydrofuran; methanol; dichloromethane; water; acetonitrile;
DOI:10.1021/ol500788c

Reference yield:

: 10437-39-5
methyl 2-deoxy-5-O-(p-toluenesulfonyl)-α,β-D-erythro-pentofuranoside

: 1592771-10-2
C₂₃H₃₈O₅Si

Guidance literature:: Multi-step reaction with 10 steps

1: potassium tert-butylate / tetrahydrofuran / 0.75 h / 0 - 20 °C / Inert atmosphere

2: lithium triethylborohydride / tetrahydrofuran / 6.25 h / 20 - 45 °C / Inert atmosphere

3: boron trifluoride diethyl etherate / dichloromethane / 0.67 h / 0 - 20 °C / Inert atmosphere

4: 4-methyl-morpholine / dichloromethane / 2 h / 20 °C / Inert atmosphere

5: methyl iodide; sodium hydrogencarbonate / acetonitrile; water / 24 h / 20 °C

6: samarium diiodide / acetonitrile; methanol / 1 h / -20 °C / Inert atmosphere

7: Dess-Martin periodane / dichloromethane / 1.5 h / 20 °C / Inert atmosphere

8: sodium tetrahydroborate / dichloromethane; methanol / 0.5 h / -80 °C / Inert atmosphere

9: 2,6-dimethylpyridine / dichloromethane / 0.5 h / 0 °C / Inert atmosphere

10: potassium hexamethylsilazane / tetrahydrofuran; toluene / 0.5 h / 0 °C / Inert atmosphere

With 4-methyl-morpholine; 2,6-dimethylpyridine; sodium tetrahydroborate; samarium diiodide; boron trifluoride diethyl etherate; potassium tert-butylate; potassium hexamethylsilazane; lithium triethylborohydride; sodium hydrogencarbonate; Dess-Martin periodane; methyl iodide; In tetrahydrofuran; methanol; dichloromethane; water; toluene; acetonitrile; 7: |Dess-Martin Oxidation;
DOI:10.1021/ol500788c