2-tert-butoxycarbonylamino-3-(4-triisopropylsilanyloxyphenyl)propionic acid

Base Information

• Chemical Name: 2-tert-butoxycarbonylamino-3-(4-triisopropylsilanyloxyphenyl)propionic acid
• CAS No.: 956413-60-8
• Molecular Formula: C₂₃H₃₉NO₅Si
• Molecular Weight: 437.652

Synonyms:2-tert-butoxycarbonylamino-3-(4-triisopropylsilanyloxyphenyl)propionic acid

Chemical Property of 2-tert-butoxycarbonylamino-3-(4-triisopropylsilanyloxyphenyl)propionic acid

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Technology Process of 2-tert-butoxycarbonylamino-3-(4-triisopropylsilanyloxyphenyl)propionic acid

There total 1 articles about 2-tert-butoxycarbonylamino-3-(4-triisopropylsilanyloxyphenyl)propionic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(S)-methyl 2-(tert-butoxycarbonylamino)-3-(4-(triisopropylsilyloxy)phenyl)propanoate (735327-63-6) → 2-tert-butoxycarbonylamino-3-(4-triisopropylsilanyloxyphenyl)propionic acid (956413-60-8)

Guidance literature:

With potassium hydroxide; In tetrahydrofuran; at 0 - 20 ℃; for 4h;

DOI:10.1021/ja0744448

Reference yield:

C19H22BrN3O6 (956413-41-5) + 2-tert-butoxycarbonylamino-3-(4-triisopropylsilanyloxyphenyl)propionic acid (956413-60-8) → 5-(7-bromo-3-hydroxy-1-methoxymethyl-2-oxo-2,3-dihydro-1H-indol-3-yl)-2-{1-[2-tert-butoxycarbonylamino-3-(4-triisopropylsilanyloxyphenyl)propionylamino]-2-methylpropyl}oxazole-4-carboxylic acid methyl ester (956413-62-0)

Guidance literature:

With benzotriazol-1-ol; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; In N,N-dimethyl-formamide; at 20 ℃;

DOI:10.1021/ja0744448

Reference yield:

L-leucine (61-90-5,21675-61-6,25248-98-0,70-45-1) + L-phenylalanine (63-91-2,25191-15-5,658-69-5,67675-33-6) + glycine (56-40-6,18875-39-3,25718-94-9) + 2-tert-butoxycarbonylamino-3-(4-triisopropylsilanyloxyphenyl)propionic acid (956413-60-8) → (S)-2-[(S)-2-(2-{2-[(S)-2-Amino-3-(4-triisopropylsilanyloxy-phenyl)-propionylamino]-acetylamino}-acetylamino)-3-phenyl-propionylamino]-4-methyl-pentanoic acid amide

Guidance literature:

Yield given. Multistep reaction; solid phase synthesis;

DOI:10.1016/S0040-4039(98)01631-1

upstream raw materials:

(S)-methyl 2-(tert-butoxycarbonylamino)-3-(4-(triisopropylsilyloxy)phenyl)propanoate

Downstream raw materials:

5-(7-bromo-3-hydroxy-1-methoxymethyl-2-oxo-2,3-dihydro-1H-indol-3-yl)-2-{1-[2-tert-butoxycarbonylamino-3-(4-triisopropylsilanyloxyphenyl)propionylamino]-2-methylpropyl}oxazole-4-carboxylic acid methyl ester

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