2-((E)-2-(benzo[d][1,3]dioxol-5-yl)vinylthio)-5-(trifluoromethyl)phenol

Base Information

Chemical Name:2-((E)-2-(benzo[d][1,3]dioxol-5-yl)vinylthio)-5-(trifluoromethyl)phenol
CAS No.:1381775-67-2
Molecular Formula:C₁₆H₁₁F₃O₃S
Molecular Weight:340.323
Hs Code.:

Synonyms:2-((E)-2-(benzo[d][1,3]dioxol-5-yl)vinylthio)-5-(trifluoromethyl)phenol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-((E)-2-(benzo[d][1,3]dioxol-5-yl)vinylthio)-5-(trifluoromethyl)phenol

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Technology Process of 2-((E)-2-(benzo[d][1,3]dioxol-5-yl)vinylthio)-5-(trifluoromethyl)phenol

There total 2 articles about 2-((E)-2-(benzo[d][1,3]dioxol-5-yl)vinylthio)-5-(trifluoromethyl)phenol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: C₇H₅F₃OS

: 17207-73-7,77150-95-9,150357-72-5
2-bromo-1-[3,4-methylenedioxyphenyl]ethylene

: 1381775-67-2
2-((E)-2-(benzo[d][1,3]dioxol-5-yl)vinylthio)-5-(trifluoromethyl)phenol

Guidance literature:: With copper(l) iodide; 1-(2-hydroxyphenyl)-3-dimethylaminoprop-2-enone; caesium carbonate; In dimethyl sulfoxide; at 100 ℃; for 24h; regioselective reaction; Inert atmosphere;
DOI:10.1016/j.tet.2012.04.048

Reference yield:

: 2373-80-0,38489-76-8
3,4-(methylenedioxy)cinnamic acid

: 1381775-67-2
2-((E)-2-(benzo[d][1,3]dioxol-5-yl)vinylthio)-5-(trifluoromethyl)phenol

Guidance literature:: Multi-step reaction with 2 steps

1.1: lithium acetate / water; acetonitrile / 0.08 h / 20 °C

1.2: 20 °C

2.1: copper(l) iodide; 1-(2-hydroxyphenyl)-3-dimethylaminoprop-2-enone; caesium carbonate / dimethyl sulfoxide / 24 h / 100 °C / Inert atmosphere

With copper(l) iodide; 1-(2-hydroxyphenyl)-3-dimethylaminoprop-2-enone; lithium acetate; caesium carbonate; In water; dimethyl sulfoxide; acetonitrile;
DOI:10.1016/j.tet.2012.04.048