C₂₉H₃₄BrClO₁₀

Base Information

Chemical Name:C₂₉H₃₄BrClO₁₀
CAS No.:1583253-32-0
Molecular Formula:C₂₉H₃₄BrClO₁₀
Molecular Weight:657.94
Hs Code.:

C<sub>29</sub>H<sub>34</sub>BrClO<sub>10</sub>

Synonyms:C₂₉H₃₄BrClO₁₀

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Chemical Property of C₂₉H₃₄BrClO₁₀

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Technology Process of C₂₉H₃₄BrClO₁₀

There total 12 articles about C₂₉H₃₄BrClO₁₀ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 2186-92-7
p-Anisaldehyde dimethyl acetal

: 1583253-30-8
C₂₁H₂₈BrClO₉

: 1583253-32-0
C₂₉H₃₄BrClO₁₀

Guidance literature:: With toluene-4-sulfonic acid; In dichloromethane; at 20 ℃; for 1h;
DOI:10.1021/ja5013307

Reference yield:

: 1583253-08-0
C₇H₁₀BrClO

: 1583253-32-0
C₂₉H₃₄BrClO₁₀

Guidance literature:: Multi-step reaction with 7 steps

1: C₁₄H₂₀N₂O₄S; chromium dichloride; zirconocene dichloride; lithium chloride; NiCl₂*2,9-dimethyl-1,10-phenanthroline complex; manganese / acetonitrile / 21 h / 20 °C / Glovebox

2: Dess-Martin periodane; sodium hydrogencarbonate / dichloromethane / 1 h / 20 °C

3: pyridine hydrogenfluoride; pyridine / acetonitrile / 16 h / 20 °C

4: 3,3-dimethyldioxirane / acetone / 0.25 h / 0 °C

5: camphor-10-sulfonic acid / dichloromethane / 0.08 h / 20 °C

6: pyridine hydrogenfluoride / acetonitrile / 3 h / 20 °C

7: toluene-4-sulfonic acid / dichloromethane / 1 h / 20 °C

With pyridine; chromium dichloride; manganese; zirconocene dichloride; C₁₄H₂₀N₂O₄S; camphor-10-sulfonic acid; NiCl₂*2,9-dimethyl-1,10-phenanthroline complex; 3,3-dimethyldioxirane; sodium hydrogencarbonate; Dess-Martin periodane; toluene-4-sulfonic acid; pyridine hydrogenfluoride; lithium chloride; In dichloromethane; acetone; acetonitrile;
DOI:10.1021/ja5013307

Reference yield:

: 1583253-15-9
C₃₉H₇₂BrClO₈Si₃

: 1583253-32-0
C₂₉H₃₄BrClO₁₀

Guidance literature:: Multi-step reaction with 6 steps

1: Dess-Martin periodane; sodium hydrogencarbonate / dichloromethane / 1 h / 20 °C

2: pyridine hydrogenfluoride; pyridine / acetonitrile / 16 h / 20 °C

3: 3,3-dimethyldioxirane / acetone / 0.25 h / 0 °C

4: camphor-10-sulfonic acid / dichloromethane / 0.08 h / 20 °C

5: pyridine hydrogenfluoride / acetonitrile / 3 h / 20 °C

6: toluene-4-sulfonic acid / dichloromethane / 1 h / 20 °C

With pyridine; camphor-10-sulfonic acid; 3,3-dimethyldioxirane; sodium hydrogencarbonate; Dess-Martin periodane; toluene-4-sulfonic acid; pyridine hydrogenfluoride; In dichloromethane; acetone; acetonitrile;
DOI:10.1021/ja5013307