C₂₈H₂₉FN₂O₆

Base Information

Chemical Name:C₂₈H₂₉FN₂O₆
CAS No.:1565781-85-2
Molecular Formula:C₂₈H₂₉FN₂O₆
Molecular Weight:508.546
Hs Code.:

C<sub>28</sub>H<sub>29</sub>FN<sub>2</sub>O<sub>6</sub>

Synonyms:C₂₈H₂₉FN₂O₆

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Chemical Property of C₂₈H₂₉FN₂O₆

Chemical Property:

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Technology Process of C₂₈H₂₉FN₂O₆

There total 10 articles about C₂₈H₂₉FN₂O₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₂₈H₂₇FN₂O₆

: 1565781-85-2
C₂₈H₂₉FN₂O₆

Guidance literature:: With sodium tetrahydroborate; In tetrahydrofuran; methanol; at 20 ℃; for 0.75h;

Reference yield:

: 847547-91-5
2-chloro-3-hydroxyquinoline-4-carboxylic acid

: 1565781-85-2
C₂₈H₂₉FN₂O₆

Guidance literature:: Multi-step reaction with 9 steps

1: methanol; toluene / Cooling with ice

2: tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate / water; ethanol; toluene / 6 h / 100 °C / Sealed tube; Inert atmosphere

3: diisobutylaluminium hydride / dichloromethane; toluene / 2.5 h / -78 - 20 °C

4: sodium hydrogencarbonate; Dess-Martin periodane / dichloromethane / 1.5 h / 20 °C

5: tetrahydrofuran / 0 °C

6: sodium hydrogencarbonate; Dess-Martin periodane / dichloromethane / 20 °C

7: boron tribromide / dichloromethane / 1 h / 20 °C

8: pyrrolidine / methanol / 8 h / 100 °C / Molecular sieve; Sealed tube

9: sodium tetrahydroborate / tetrahydrofuran; methanol / 0.75 h / 20 °C

With pyrrolidine; sodium tetrahydroborate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; boron tribromide; diisobutylaluminium hydride; sodium hydrogencarbonate; potassium carbonate; Dess-Martin periodane; In tetrahydrofuran; methanol; ethanol; dichloromethane; water; toluene;

Reference yield:

: 1565779-05-6
C₁₂H₁₀ClNO₃

: 1565781-85-2
C₂₈H₂₉FN₂O₆

Guidance literature:: Multi-step reaction with 8 steps

1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate / water; ethanol; toluene / 6 h / 100 °C / Sealed tube; Inert atmosphere

2: diisobutylaluminium hydride / dichloromethane; toluene / 2.5 h / -78 - 20 °C

3: sodium hydrogencarbonate; Dess-Martin periodane / dichloromethane / 1.5 h / 20 °C

4: tetrahydrofuran / 0 °C

5: sodium hydrogencarbonate; Dess-Martin periodane / dichloromethane / 20 °C

6: boron tribromide / dichloromethane / 1 h / 20 °C

7: pyrrolidine / methanol / 8 h / 100 °C / Molecular sieve; Sealed tube

8: sodium tetrahydroborate / tetrahydrofuran; methanol / 0.75 h / 20 °C

With pyrrolidine; sodium tetrahydroborate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; boron tribromide; diisobutylaluminium hydride; sodium hydrogencarbonate; potassium carbonate; Dess-Martin periodane; In tetrahydrofuran; methanol; ethanol; dichloromethane; water; toluene;