Technology Process of C18H20INO6S
There total 7 articles about C18H20INO6S which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
trifluoroacetic acid;
In
dichloromethane;
at 20 ℃;
for 24h;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: silver trifluoroacetate; iodine / chloroform / 120 h / -60 °C
2: tetrabutyl ammonium fluoride / tetrahydrofuran / 1 h / 0 °C
3: potassium carbonate / acetone / 21 h / Reflux
4: trifluoroacetic acid / dichloromethane / 24 h / 20 °C
With
tetrabutyl ammonium fluoride; iodine; silver trifluoroacetate; potassium carbonate; trifluoroacetic acid;
In
tetrahydrofuran; dichloromethane; chloroform; acetone;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: tetrabutyl ammonium fluoride / tetrahydrofuran / 1 h / 0 °C
2: potassium carbonate / acetone / 21 h / Reflux
3: trifluoroacetic acid / dichloromethane / 24 h / 20 °C
With
tetrabutyl ammonium fluoride; potassium carbonate; trifluoroacetic acid;
In
tetrahydrofuran; dichloromethane; acetone;