4-methyl-2-{(E)-[(R)-1-phenylethylimino]methyl}-6-{(1S,2R,4R)-1,7,7-trimethylbiyclo[2.2.1]hept-exo-2-yl}phenol

Base Information

• Chemical Name: 4-methyl-2-{(E)-[(R)-1-phenylethylimino]methyl}-6-{(1S,2R,4R)-1,7,7-trimethylbiyclo[2.2.1]hept-exo-2-yl}phenol
• CAS No.: 1193126-51-0
• Molecular Formula: C₂₆H₃₃NO
• Molecular Weight: 375.554

Synonyms:4-methyl-2-{(E)-[(R)-1-phenylethylimino]methyl}-6-{(1S,2R,4R)-1,7,7-trimethylbiyclo[2.2.1]hept-exo-2-yl}phenol

Chemical Property of 4-methyl-2-{(E)-[(R)-1-phenylethylimino]methyl}-6-{(1S,2R,4R)-1,7,7-trimethylbiyclo[2.2.1]hept-exo-2-yl}phenol

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Technology Process of 4-methyl-2-{(E)-[(R)-1-phenylethylimino]methyl}-6-{(1S,2R,4R)-1,7,7-trimethylbiyclo[2.2.1]hept-exo-2-yl}phenol

There total 1 articles about 4-methyl-2-{(E)-[(R)-1-phenylethylimino]methyl}-6-{(1S,2R,4R)-1,7,7-trimethylbiyclo[2.2.1]hept-exo-2-yl}phenol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

2-hydroxy-5-methyl-3-(1,7,7-trimethylbiyclo[2.2.1]hept-exo-2-yl)benzaldehyde (1174375-65-5) + (R)-1-phenyl-ethyl-amine (3886-69-9) → 4-methyl-2-{(E)-[(R)-1-phenylethylimino]methyl}-6-{(1R,2S,4S)-1,7,7-trimethylbiyclo[2.2.1]hept-exo-2-yl}phenol (1193126-49-6) + 4-methyl-2-{(E)-[(R)-1-phenylethylimino]methyl}-6-{(1S,2R,4R)-1,7,7-trimethylbiyclo[2.2.1]hept-exo-2-yl}phenol (1193126-51-0)

Guidance literature:

With triethylamine; In toluene; for 3.5h; optical yield given as %de; Molecular sieve; Inert atmosphere; Reflux;

DOI:10.1134/S1070428010050088

Reference yield: 97.0%

4-methyl-2-{(E)-[(R)-1-phenylethylimino]methyl}-6-{(1S,2R,4R)-1,7,7-trimethylbiyclo[2.2.1]hept-exo-2-yl}phenol (1193126-51-0) → 2-hydroxy-5-methyl-3-((1S,2R,4R)-1,7,7-trimethylbicyclo[2.2.1]hept-exo-2-yl)benzaldehyde

Guidance literature:

With hydrogenchloride; In ethanol; water; at 20 ℃; for 6h; optical yield given as %ee;

DOI:10.1134/S1070428010050088

upstream raw materials:

2-hydroxy-5-methyl-3-(1,7,7-trimethylbiyclo[2.2.1]hept-exo-2-yl)benzaldehyde

(R)-1-phenyl-ethyl-amine

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