3-(5,6-dimethyl-1H-benzo[d]imidazol-2-yl)-1-(4-methoxyphenyl)-9H-pyrido[3,4-b]indole

Base Information

Chemical Name:3-(5,6-dimethyl-1H-benzo[d]imidazol-2-yl)-1-(4-methoxyphenyl)-9H-pyrido[3,4-b]indole
CAS No.:1585210-60-1
Molecular Formula:C₂₇H₂₂N₄O
Molecular Weight:418.498
Hs Code.:

Synonyms:3-(5,6-dimethyl-1H-benzo[d]imidazol-2-yl)-1-(4-methoxyphenyl)-9H-pyrido[3,4-b]indole

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Chemical Property of 3-(5,6-dimethyl-1H-benzo[d]imidazol-2-yl)-1-(4-methoxyphenyl)-9H-pyrido[3,4-b]indole

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Technology Process of 3-(5,6-dimethyl-1H-benzo[d]imidazol-2-yl)-1-(4-methoxyphenyl)-9H-pyrido[3,4-b]indole

There total 6 articles about 3-(5,6-dimethyl-1H-benzo[d]imidazol-2-yl)-1-(4-methoxyphenyl)-9H-pyrido[3,4-b]indole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 1585210-51-0
1-(4-methoxyphenyl)-9H-pyrido[3,4-b]indole-3-carbaldehyde

: 3171-45-7
4,5-dimethyl-1,2-phenylenediamine

: 1585210-60-1
3-(5,6-dimethyl-1H-benzo[d]imidazol-2-yl)-1-(4-methoxyphenyl)-9H-pyrido[3,4-b]indole

Guidance literature:: With lanthanum(III) nitrate hexahydrate; In ethanol; for 0.5h; chemoselective reaction; Heating;
DOI:10.1039/c3ob42236d

Reference yield:

: 73-22-3,27732-43-0,80206-30-0,27813-82-7
L-Tryptophan

: 1585210-60-1
3-(5,6-dimethyl-1H-benzo[d]imidazol-2-yl)-1-(4-methoxyphenyl)-9H-pyrido[3,4-b]indole

Guidance literature:: Multi-step reaction with 6 steps

1: thionyl chloride / 6 h / 0 - 20 °C

2: toluene-4-sulfonic acid / toluene / 24 h / Reflux

3: sulfur / 5,5-dimethyl-1,3-cyclohexadiene / 12 h / Reflux

4: lithium aluminium tetrahydride / tetrahydrofuran / 4 h / -5 - 20 °C

5: Dess-Martin periodane / dichloromethane / 2 h / 20 °C

6: lanthanum(III) nitrate hexahydrate / ethanol / 0.5 h / Heating

With lithium aluminium tetrahydride; thionyl chloride; lanthanum(III) nitrate hexahydrate; Dess-Martin periodane; toluene-4-sulfonic acid; sulfur; In tetrahydrofuran; 5,5-dimethyl-1,3-cyclohexadiene; ethanol; dichloromethane; toluene;
DOI:10.1039/c3ob42236d

Reference yield:

: 4299-70-1
L-tryptophan methyl ester

: 1585210-60-1
3-(5,6-dimethyl-1H-benzo[d]imidazol-2-yl)-1-(4-methoxyphenyl)-9H-pyrido[3,4-b]indole

Guidance literature:: Multi-step reaction with 5 steps

1: toluene-4-sulfonic acid / toluene / 24 h / Reflux

2: sulfur / 5,5-dimethyl-1,3-cyclohexadiene / 12 h / Reflux

3: lithium aluminium tetrahydride / tetrahydrofuran / 4 h / -5 - 20 °C

4: Dess-Martin periodane / dichloromethane / 2 h / 20 °C

5: lanthanum(III) nitrate hexahydrate / ethanol / 0.5 h / Heating

With lithium aluminium tetrahydride; lanthanum(III) nitrate hexahydrate; Dess-Martin periodane; toluene-4-sulfonic acid; sulfur; In tetrahydrofuran; 5,5-dimethyl-1,3-cyclohexadiene; ethanol; dichloromethane; toluene;
DOI:10.1039/c3ob42236d